((2R,3R,4S,5R,6R)-4-Benzyloxy-6-isobutoxy-5-isopropoxy-2-trifluoromethanesulfonyloxymethyl-tetrahydro-pyran-3-yloxy)-acetic acid tert-butyl ester

Base Information

Chemical Name:((2R,3R,4S,5R,6R)-4-Benzyloxy-6-isobutoxy-5-isopropoxy-2-trifluoromethanesulfonyloxymethyl-tetrahydro-pyran-3-yloxy)-acetic acid tert-butyl ester
CAS No.:182418-26-4
Molecular Formula:C₂₇H₄₁F₃O₁₀S
Molecular Weight:614.678
Hs Code.:

((2R,3R,4S,5R,6R)-4-Benzyloxy-6-isobutoxy-5-isopropoxy-2-trifluoromethanesulfonyloxymethyl-tetrahydro-pyran-3-yloxy)-acetic acid tert-butyl ester

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Chemical Property of ((2R,3R,4S,5R,6R)-4-Benzyloxy-6-isobutoxy-5-isopropoxy-2-trifluoromethanesulfonyloxymethyl-tetrahydro-pyran-3-yloxy)-acetic acid tert-butyl ester

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Technology Process of ((2R,3R,4S,5R,6R)-4-Benzyloxy-6-isobutoxy-5-isopropoxy-2-trifluoromethanesulfonyloxymethyl-tetrahydro-pyran-3-yloxy)-acetic acid tert-butyl ester

There total 9 articles about ((2R,3R,4S,5R,6R)-4-Benzyloxy-6-isobutoxy-5-isopropoxy-2-trifluoromethanesulfonyloxymethyl-tetrahydro-pyran-3-yloxy)-acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18685-18-2
3-O-benzyl-1,2-5,6-O-diisopropylidene-α-D-glucofuranose

: 182418-26-4
((2R,3R,4S,5R,6R)-4-Benzyloxy-6-isobutoxy-5-isopropoxy-2-trifluoromethanesulfonyloxymethyl-tetrahydro-pyran-3-yloxy)-acetic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 11 steps

1: 1) H⁽¹⁺⁾, 2) pyridine

2: 1) TiBr₄, 2) HgO, HgBr, CaSO₄ / 1) CHCl₃

3: NaOMe, MeOH

4: pTSA / acetonitrile

5: pyridine

6: 1), 2) H₂ / 2) Pd/BaSO₄

7: I₂, MeOH

8: pyridine / Heating

9: NaH, DMF

10: acidic ion-exchange resin / methanol

11: pyridine / CH₂Cl₂

With pyridine; methanol; calcium sulfate; acidic ion-exchange resin; hydrogen; iodine; sodium methylate; mercury(I) bromide; hydrogen cation; titanium(IV) bromide; sodium hydride; toluene-4-sulfonic acid; N,N-dimethyl-formamide; mercury(II) oxide; Pd-BaSO₄; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/0960-894X(96)00336-8

Reference yield:

: 182417-82-9
(2R,4aR,6R,7R,8R,8aR)-8-Benzyloxy-6-isobutoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ol

: 182418-26-4
((2R,3R,4S,5R,6R)-4-Benzyloxy-6-isobutoxy-5-isopropoxy-2-trifluoromethanesulfonyloxymethyl-tetrahydro-pyran-3-yloxy)-acetic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine

2: 1), 2) H₂ / 2) Pd/BaSO₄

3: I₂, MeOH

4: pyridine / Heating

5: NaH, DMF

6: acidic ion-exchange resin / methanol

7: pyridine / CH₂Cl₂

With pyridine; methanol; acidic ion-exchange resin; hydrogen; iodine; sodium hydride; N,N-dimethyl-formamide; Pd-BaSO₄; In methanol; dichloromethane;
DOI:10.1016/0960-894X(96)00336-8

Reference yield:

: 182698-05-1
C₄₁H₃₄O₁₀

: 182418-26-4
((2R,3R,4S,5R,6R)-4-Benzyloxy-6-isobutoxy-5-isopropoxy-2-trifluoromethanesulfonyloxymethyl-tetrahydro-pyran-3-yloxy)-acetic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 10 steps

1: 1) TiBr₄, 2) HgO, HgBr, CaSO₄ / 1) CHCl₃

2: NaOMe, MeOH

3: pTSA / acetonitrile

4: pyridine

5: 1), 2) H₂ / 2) Pd/BaSO₄

6: I₂, MeOH

7: pyridine / Heating

8: NaH, DMF

9: acidic ion-exchange resin / methanol

10: pyridine / CH₂Cl₂

With pyridine; methanol; calcium sulfate; acidic ion-exchange resin; hydrogen; iodine; sodium methylate; mercury(I) bromide; titanium(IV) bromide; sodium hydride; toluene-4-sulfonic acid; N,N-dimethyl-formamide; mercury(II) oxide; Pd-BaSO₄; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/0960-894X(96)00336-8