Technology Process of 4-(octadeca-10,12-diynoyloxy)benzylidenemalononitrile
There total 4 articles about 4-(octadeca-10,12-diynoyloxy)benzylidenemalononitrile which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
tetrahydrofuran;
for 2h;
Heating;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 60 percent / 10percent aq. potassium hydroxide, hydroxylamine hydrochloride, cuprous chloride, butylamine / methanol; tetrahydrofuran / 2 h
2: 83 percent / thionyl chloride / petroleum ether / 3 h / Heating
3: 78 percent / triethylamine / tetrahydrofuran / 2 h / Heating
With
potassium hydroxide; thionyl chloride; hydroxylamine hydrochloride; N-butylamine; triethylamine; copper(l) chloride;
In
tetrahydrofuran; methanol; Petroleum ether;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 60 percent / 10percent aq. potassium hydroxide, hydroxylamine hydrochloride, cuprous chloride, butylamine / methanol; tetrahydrofuran / 2 h
2: 83 percent / thionyl chloride / petroleum ether / 3 h / Heating
3: 78 percent / triethylamine / tetrahydrofuran / 2 h / Heating
With
potassium hydroxide; thionyl chloride; hydroxylamine hydrochloride; N-butylamine; triethylamine; copper(l) chloride;
In
tetrahydrofuran; methanol; Petroleum ether;
