rac-cyclohexane-1,2,3-triyl triacetate

Base Information

• Chemical Name: rac-cyclohexane-1,2,3-triyl triacetate
• CAS No.: 62365-17-7
• Molecular Formula: C₁₂H₁₈O₆
• Molecular Weight: 258.271
• Mol file: 62365-17-7.mol

Synonyms:

Chemical Property of rac-cyclohexane-1,2,3-triyl triacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of rac-cyclohexane-1,2,3-triyl triacetate

There total 4 articles about rac-cyclohexane-1,2,3-triyl triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

rac-cyclohexane-1,2,3-triol (2630-65-1,6286-43-7,10515-21-6,13302-87-9,62445-01-6,123163-99-5,2630-64-0) + acetic anhydride (108-24-7) → rac-cyclohexane-1,2,3-triyl triacetate (20021-58-3,62365-17-7,92935-79-0)

Guidance literature:

rac-cyclohexane-1,2,3-triol; With pyridine; at 0 ℃; for 0.5h;

acetic anhydride; at 20 ℃;

DOI:10.1055/s-0029-1217965

Reference yield:

rac-3-acetoxycyclohexene (76644-52-5,76704-31-9,14447-34-8,62247-41-0) → Tri-O-acetyl-all-cis-cyclohexantriol-(1,2,3) (20021-58-3,62365-17-7,92935-79-0)

Guidance literature:

Multi-step reaction with 2 steps

1: N-methylmorpholine N-oxide monohydrate, OsO₄ / methanol; acetone; 2-methyl-propan-2-ol / Ambient temperature

With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In methanol; acetone; tert-butyl alcohol;

DOI:10.1016/0040-4020(84)80008-3

Reference yield:

rac-3-acetoxycyclohexene (76644-52-5,76704-31-9,14447-34-8,62247-41-0) → rac-cyclohexane-1,2,3-triyl triacetate (20021-58-3,62365-17-7,92935-79-0)

Guidance literature:

Multi-step reaction with 2 steps

1: N-methylmorpholine N-oxide monohydrate, OsO₄ / methanol; acetone; 2-methyl-propan-2-ol / Ambient temperature

With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In methanol; acetone; tert-butyl alcohol;

DOI:10.1016/0040-4020(84)80008-3

upstream raw materials:

rac-3-acetoxycyclohexene

rac-cyclohexane-1,2,3-triol

acetic anhydride