rac.-β-Phenyl-β-deutero-buttersaeure

Base Information

• Chemical Name: rac.-β-Phenyl-β-deutero-buttersaeure
• CAS No.: 16428-64-1
• Molecular Formula: C₁₀H₁₂O₂
• Molecular Weight: 165.196
• Mol file: 16428-64-1.mol

Synonyms:

Chemical Property of rac.-β-Phenyl-β-deutero-buttersaeure

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of rac.-β-Phenyl-β-deutero-buttersaeure

There total 4 articles about rac.-β-Phenyl-β-deutero-buttersaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Phenyl-1-butanol-3-d (226958-61-8) → rac.-β-Phenyl-β-deutero-buttersaeure (16428-64-1)

Guidance literature:

With potassium permanganate; dipotassium hydrogenphosphate; potassium dihydrogenphosphate; for 48h;

DOI:10.1021/ja01044a024

Reference yield:

(E)-3-phenyl-2-butenoic acid (704-80-3) → rac.-β-Phenyl-β-deutero-buttersaeure (16428-64-1)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) LiAlH₄, (ii) D₂O

2: KMnO₄, KH₂PO₄, K₂HPO₄ / 48 h

With potassium permanganate; dipotassium hydrogenphosphate; potassium dihydrogenphosphate;

DOI:10.1021/ja01044a024

Reference yield:

3-phenylbut-2-enoic acid (704-79-0,704-80-3,1199-20-8) → rac.-β-Phenyl-β-deutero-buttersaeure (16428-64-1)

Guidance literature:

Multistep reaction; (i) LiAlH₄, (ii) D₂O, (iii) KMnO₄;

DOI:10.1021/ja01001a600

upstream raw materials:

3-Phenyl-1-butanol-3-d

3-phenylbut-2-enoic acid

(E)-3-phenyl-2-butenoic acid

Downstream raw materials:

(-)-β-Phenyl-β-deutero-buttersaeure

(+)-β-Phenyl-β-deutero-buttersaeure