Boc-L-2-amino-6-(O,O'-diethyl-phosphono)hexanoicacid

Base Information

Chemical Name:Boc-L-2-amino-6-(O,O'-diethyl-phosphono)hexanoicacid
CAS No.:1217810-32-6
Molecular Formula:C₁₅H₃₀NO₇P
Molecular Weight:367.379
Hs Code.:
Mol file:1217810-32-6.mol

Synonyms:

Suppliers and Price of Boc-L-2-amino-6-(O,O'-diethyl-phosphono)hexanoicacid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
Boc-L-2-amino-6-(O,O'-diethyl-phosphono)hexanoicacid
250mg
$ 814.00

Matrix Scientific
Boc-L-2-amino-6-(O,O'-diethyl-phosphono)hexanoicacid
100mg
$ 446.00

American Custom Chemicals Corporation
BOC-L-2-AMINO-6-(O,O'-DIETHYL-PHOSPHONO)HEXANOIC ACID 95.00%
250MG
$ 1472.63

American Custom Chemicals Corporation
BOC-L-2-AMINO-6-(O,O'-DIETHYL-PHOSPHONO)HEXANOIC ACID 95.00%
100MG
$ 773.85

Total 1 raw suppliers

Chemical Property of Boc-L-2-amino-6-(O,O'-diethyl-phosphono)hexanoicacid

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

Boc-L-2-amino-6-(O,O'-diethyl-phosphono)hexanoicacid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Boc-L-2-amino-6-(O,O'-diethyl-phosphono)hexanoicacid

There total 10 articles about Boc-L-2-amino-6-(O,O'-diethyl-phosphono)hexanoicacid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: (R)-tert-butyl (6-(diethoxyphosphoryl)-1-hydroxyhexan-2-yl)carbamate

: 1217810-32-6
(R)-2-((tert-butoxycarbonyl)amino)-6-(diethoxyphosphoryl)hexanoic acid

Guidance literature:: (R)-tert-butyl (6-(diethoxyphosphoryl)-1-hydroxyhexan-2-yl)carbamate; With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In water; acetonitrile; at 0 ℃; for 0.0833333h;

With sodium hydrogencarbonate; In water; acetonitrile; at 0 ℃; for 2h;
DOI:10.1002/chem.201700604

Reference yield: 80.0%

: (S)-tert-butyl (6-(diethoxyphosphoryl)-1-hydroxyhexan-2-yl)carbamate

: 1217810-32-6
(S)-2-((tert-butoxycarbonyl)amino)-6-(diethoxyphosphoryl)hexanoic acid

Guidance literature:: (S)-tert-butyl (6-(diethoxyphosphoryl)-1-hydroxyhexan-2-yl)carbamate; With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In water; acetonitrile; at 0 ℃; for 0.0833333h;

With sodium hydrogencarbonate; In water; acetonitrile; at 0 ℃; for 2h;
DOI:10.1002/chem.201700604

Reference yield:

: (R)-tert-butyl 4-(4-(diethoxyphosphoryl)but-3-en-1-yl)-2,2-dimethyloxazolidine-3-carboxylate

: 1217810-32-6
(R)-2-((tert-butoxycarbonyl)amino)-6-(diethoxyphosphoryl)hexanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: palladium 10% on activated carbon; hydrogen / ethanol / 2 h / 20 °C

2.1: toluene-4-sulfonic acid / methanol / 6 h / 20 °C

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / acetonitrile; water / 0.08 h / 0 °C

3.2: 2 h / 0 °C

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; hydrogen; toluene-4-sulfonic acid; In methanol; ethanol; water; acetonitrile;
DOI:10.1002/chem.201700604