C₂₂H₃₈N₂O₅Si

Base Information

• Chemical Name: C₂₂H₃₈N₂O₅Si
• CAS No.: 1446101-10-5
• Molecular Formula: C₂₂H₃₈N₂O₅Si
• Molecular Weight: 438.64
• Mol file: 1446101-10-5.mol

Synonyms:

Chemical Property of C₂₂H₃₈N₂O₅Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₃₈N₂O₅Si

There total 6 articles about C₂₂H₃₈N₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2S)-2-amino-N-butyl-3-(4-hydroxyphenyl)propanamide (40829-19-4) → C22H38N2O5Si (1446101-10-5)

Guidance literature:

Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / methanol / 24 h / Reflux

2: potassium carbonate / acetonitrile / Inert atmosphere

3: bi(cyclopentadienyl)platinum dichloride / tetrahydrofuran / 48 h / Inert atmosphere; Reflux

With bi(cyclopentadienyl)platinum dichloride; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; acetonitrile;

DOI:10.1021/ol401390z

Reference yield:

L-Tyr-OMe (1080-06-4) → C22H38N2O5Si (1446101-10-5)

Guidance literature:

Multi-step reaction with 4 steps

1: 24 h / 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / methanol / 24 h / Reflux

3: potassium carbonate / acetonitrile / Inert atmosphere

4: bi(cyclopentadienyl)platinum dichloride / tetrahydrofuran / 48 h / Inert atmosphere; Reflux

With bi(cyclopentadienyl)platinum dichloride; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; acetonitrile;

DOI:10.1021/ol401390z

Reference yield:

Triethoxysilane (998-30-1) + C19H28N2O2 (1364703-09-2) → C22H38N2O5Si (1446101-10-5)

Guidance literature:

With bi(cyclopentadienyl)platinum dichloride; In tetrahydrofuran; for 48h; Inert atmosphere; Reflux;

DOI:10.1021/ol401390z

upstream raw materials:

Triethoxysilane

C₁₉H₂₈N₂O₂

L-Tyr-OMe

(2S)-2-amino-N-butyl-3-(4-hydroxyphenyl)propanamide