[MoI₂(CO)3(CH₃C(CH₂P(C₆H₅)2)3-P,P')]

Base Information

Chemical Name:[MoI₂(CO)3(CH₃C(CH₂P(C₆H₅)2)3-P,P')]
CAS No.:20523-65-3
Molecular Formula:C₄₄H₃₉I₂MoO₃P₃
Molecular Weight:1058.46
Hs Code.:

[MoI<sub>2</sub>(CO)3(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3-P,P')]

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Suppliers and Price of [MoI₂(CO)3(CH₃C(CH₂P(C₆H₅)2)3-P,P')]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [MoI₂(CO)3(CH₃C(CH₂P(C₆H₅)2)3-P,P')]

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Technology Process of [MoI₂(CO)3(CH₃C(CH₂P(C₆H₅)2)3-P,P')]

There total 1 articles about [MoI₂(CO)3(CH₃C(CH₂P(C₆H₅)2)3-P,P')] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 102349-56-4
MoI₂(CO)3(MeCN)2

: 22031-12-5
[2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine]

: 20523-65-3
[MoI₂(CO)3(CH₃C(CH₂P(C₆H₅)2)3-P,P')]

Guidance literature:: In dichloromethane; ligand was added to Mo-complex in CH2Cl2 at 0°C, stirred for 5 min under N2; filtered, solvent was removed in vacuo, recrystd. from CH2Cl2-Et2O at -17°C; elem. anal.;
DOI:10.1016/S0022-328X(01)01367-5

Reference yield: 90.0%

: 102349-56-4
MoI₂(CO)3(MeCN)2

: 60-29-7,927820-24-4
diethyl ether

: 20523-65-3
[MoI₂(CO)3(CH₃C(CH₂P(C₆H₅)2)3-P,P')]

: 603-35-0
triphenylphosphine

: [MoI2(CO)3PPh3(μ-MoI2(CO)3(1,1,1-tris(diphenylphosphinomethyl)ethane-P,P')]*Et2O

Guidance literature:: In dichloromethane; PPh3 was added to Mo-complex in CH2Cl2 at room temp., stirred for 1 min,Mo-complex was added under N2; filtered, solvent was removed in vacuo after 24 h, recrystd. from CH2Cl2-Et2O at -17°C; elem. anal.;
DOI:10.1016/S0022-328X(01)01367-5

Reference yield: 87.0%

: 102349-56-4
MoI₂(CO)3(MeCN)2

: 60-29-7,927820-24-4
diethyl ether

: 20523-65-3
[MoI₂(CO)3(CH₃C(CH₂P(C₆H₅)2)3-P,P')]

: [MoI2(CO)3(μ-MoI2(CO)3(1,1,1-tris(diphenylphosphinomethyl)ethane-P,P')2]*2Et2O

Guidance literature:: In dichloromethane; Mo-complex was added to stireed soln. of Mo-complex in CH2Cl2 under N2; filtered, solvent was removed in vacuo after 24 h, recrystd. from CH2Cl2-Et2O at -17°C; elem. anal.;
DOI:10.1016/S0022-328X(01)01367-5