C₁₄H₁₉N

Base Information

• Chemical Name: C₁₄H₁₉N
• CAS No.: 1361023-96-2
• Molecular Formula: C₁₄H₁₉N
• Molecular Weight: 201.312

Synonyms:

Chemical Property of C₁₄H₁₉N

Chemical Property:

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Technology Process of C₁₄H₁₉N

There total 3 articles about C₁₄H₁₉N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

isovaleraldehyde (590-86-3) → C14H19N (1361023-96-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / Inert atmosphere; Cooling with acetonitrile-dry ice

2.2: Saturated solution

3.1: Milstein's PNN catalyst / ⁽²⁾H₈-toluene / 24 h / Reflux; Inert atmosphere

With Milstein's PNN catalyst; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; In tetrahydrofuran; ⁽²⁾H₈-toluene; toluene;

DOI:10.1039/c2ob06921k

Reference yield:

5-methyl-2-hexenoic acid ethyl ester (34993-63-0,79918-80-2,2351-89-5) → C14H19N (1361023-96-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / Inert atmosphere; Cooling with acetonitrile-dry ice

1.2: Saturated solution

2.1: Milstein's PNN catalyst / ⁽²⁾H₈-toluene / 24 h / Reflux; Inert atmosphere

With Milstein's PNN catalyst; diisobutylaluminium hydride; In tetrahydrofuran; ⁽²⁾H₈-toluene; toluene;

DOI:10.1039/c2ob06921k

Reference yield:

5-Methyl-2-hexen-1-ol (1589-35-1,95979-32-1,77053-92-0) + benzylamine (100-46-9) → C14H19N (1361023-96-2)

Guidance literature:

With Milstein's PNN catalyst; In ⁽²⁾H₈-toluene; for 24h; Reflux; Inert atmosphere;

DOI:10.1039/c2ob06921k

upstream raw materials:

5-Methyl-2-hexen-1-ol

benzylamine

5-methyl-2-hexenoic acid ethyl ester

isovaleraldehyde

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