C₃₂H₄₅N₃O₇

Base Information

• Chemical Name: C₃₂H₄₅N₃O₇
• CAS No.: 1070503-96-6
• Molecular Formula: C₃₂H₄₅N₃O₇
• Molecular Weight: 583.725
• Mol file: 1070503-96-6.mol

Synonyms:

Chemical Property of C₃₂H₄₅N₃O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₂H₄₅N₃O₇

There total 8 articles about C₃₂H₄₅N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

C39H51N3O7 (1070503-95-5) → C32H45N3O7 (1070503-96-6)

Guidance literature:

With ammonium acetate; palladium;

DOI:10.1002/chem.201103605

Reference yield:

4-bromosalicylaldehyde (22532-62-3) → C32H45N3O7 (1070503-96-6)

Guidance literature:

Multi-step reaction with 9 steps

1.1: potassium carbonate

2.1: sodium methylate / methanol

2.2: 160 °C

3.1: sodium hydroxide / water

3.3: 215 °C

4.1: trichlorophosphate / N,N-dimethyl-formamide

5.1: ammonium acetate

6.1: lithium aluminium tetrahydride

7.1: dmap

8.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) chloride; lithium chloride

9.1: ammonium acetate; palladium

With dmap; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium acetate; sodium methylate; potassium carbonate; palladium; copper(l) chloride; lithium chloride; sodium hydroxide; trichlorophosphate; In methanol; water; N,N-dimethyl-formamide; 2.1: Hemetsberger indole cyclization / 5.1: Henry reaction;

DOI:10.1002/chem.201103605

Reference yield:

2-(benzyloxy)-4-bromobenzaldehyde (142602-43-5) → C32H45N3O7 (1070503-96-6)

Guidance literature:

Multi-step reaction with 8 steps

1.1: sodium methylate / methanol

1.2: 160 °C

2.1: sodium hydroxide / water

2.3: 215 °C

3.1: trichlorophosphate / N,N-dimethyl-formamide

4.1: ammonium acetate

5.1: lithium aluminium tetrahydride

6.1: dmap

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) chloride; lithium chloride

8.1: ammonium acetate; palladium

With dmap; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium acetate; sodium methylate; palladium; copper(l) chloride; lithium chloride; sodium hydroxide; trichlorophosphate; In methanol; water; N,N-dimethyl-formamide; 1.1: Hemetsberger indole cyclization / 4.1: Henry reaction;

DOI:10.1002/chem.201103605

upstream raw materials:

C₃₉H₅₁N₃O₇

C₂₇H₃₃BrN₂O₅

C₁₇H₁₃BrN₂O₃

C₁₆H₁₂BrNO₂

Downstream raw materials:

C₂₇H₃₅N₃O₆

C₂₇H₃₅N₃O₆

C₃₂H₄₃N₃O₈

Refernces