Technology Process of C18H27N3O5*ClH
There total 9 articles about C18H27N3O5*ClH which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium on activated charcoal; hydrogen / methanol / 10 h / 760.05 Torr
2: hydrogenchloride / ethyl acetate / 12 h / 0 °C
With
hydrogenchloride; palladium on activated charcoal; hydrogen;
In
methanol; ethyl acetate;
DOI:10.3109/14756361003698147
- Guidance literature:
-
Multi-step reaction with 8 steps
1: sodium hydroxide / methanol
2: tetra-(n-butyl)ammonium iodide; potassium carbonate; potassium iodide / acetone
3: hydrogenchloride / ethyl acetate
4: dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 13 h / 0 - 20 °C
5: hydrogenchloride / ethyl acetate / 7 h / 0 - 20 °C
6: dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 13 h / 0 - 20 °C
7: palladium on activated charcoal; hydrogen / methanol / 10 h / 760.05 Torr
8: hydrogenchloride / ethyl acetate / 12 h / 0 °C
With
hydrogenchloride; dmap; palladium on activated charcoal; hydrogen; tetra-(n-butyl)ammonium iodide; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium iodide; sodium hydroxide;
In
methanol; dichloromethane; ethyl acetate; acetone;
DOI:10.3109/14756361003698147
