C₅₄H₄₂N₂

Base Information

Chemical Name:C₅₄H₄₂N₂
CAS No.:338992-56-6
Molecular Formula:C₅₄H₄₂N₂
Molecular Weight:718.941
Hs Code.:

C<sub>54</sub>H<sub>42</sub>N<sub>2</sub>

Synonyms:

Suppliers and Price of C₅₄H₄₂N₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₄H₄₂N₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₄H₄₂N₂

There total 10 articles about C₅₄H₄₂N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: C₄₇H₅₅NP⁽¹⁺⁾*Br^(1-)

: 4181-05-9
4-(diphenylamino)benzaldehyde

: 338992-56-6
C₅₄H₄₂N₂

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 3h; Reflux;
DOI:10.1021/ja309393c

Reference yield:

: 603-34-9
N,N-diphenylaminobenzene

: 338992-56-6
C₅₄H₄₂N₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: trichlorophosphate / 2 h / 45 - 50 °C

2.1: sodium tetrahydroborate / dichloromethane; methanol / 2 h / 20 °C

3.1: phosphorus tribromide / diethyl ether / 15 h / 0 - 20 °C

4.1: toluene / 24 h / Reflux

5.1: potassium tert-butylate / tetrahydrofuran / 3.67 h / Inert atmosphere; Reflux

5.2: 15 h / 0 - 20 °C / Inert atmosphere

6.1: sodium hydroxide; sodium tetrahydroborate / tetrahydrofuran; methanol; water / 15 h / 20 °C

7.1: phosphorus tribromide / tetrahydrofuran; diethyl ether / 15 h / 0 - 20 °C

8.1: toluene / 16 h / Reflux

9.1: potassium tert-butylate / tetrahydrofuran / 3.4 h / Inert atmosphere; Reflux

9.2: 15 h / 0 - 20 °C / Inert atmosphere

10.1: sodium hydroxide; sodium tetrahydroborate / tetrahydrofuran; methanol; water / 15 h / 20 °C

10.2: 15 h / 0 - 20 °C

11.1: toluene / 24 h / Reflux

12.1: potassium tert-butylate / tetrahydrofuran / 3 h / Reflux

With sodium tetrahydroborate; potassium tert-butylate; phosphorus tribromide; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; 12.1: |Wittig Olefination;
DOI:10.1021/ja309393c

Reference yield:

: 1229113-74-9
C₂₇H₂₂BrN

: 338992-56-6
C₅₄H₄₂N₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene / 16 h / Reflux

2.1: potassium tert-butylate / tetrahydrofuran / 3.4 h / Inert atmosphere; Reflux

2.2: 15 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydroxide; sodium tetrahydroborate / tetrahydrofuran; methanol; water / 15 h / 20 °C

3.2: 15 h / 0 - 20 °C

4.1: toluene / 24 h / Reflux

5.1: potassium tert-butylate / tetrahydrofuran / 3 h / Reflux

With sodium tetrahydroborate; potassium tert-butylate; sodium hydroxide; In tetrahydrofuran; methanol; water; toluene; 5.1: |Wittig Olefination;
DOI:10.1021/ja309393c