Technology Process of C7H6O2*C9H14N2O
There total 7 articles about C7H6O2*C9H14N2O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium tetrahydroborate; methanol / tetrahydrofuran / -4 - 27 °C / Inert atmosphere
2.1: triethylamine / dichloromethane / -6 - 20 °C / Inert atmosphere
3.1: sodium hydride / 1-methyl-pyrrolidin-2-one; mineral oil / 1.5 h / 5 - 20 °C / Inert atmosphere
3.2: 3 h / 68 °C
4.1: ammonium formate / palladium 10% on activated carbon / ethanol / 15.5 h / 60 - 71 °C / Inert atmosphere
5.1: water; Isopropyl acetate / 60 °C
With
methanol; sodium tetrahydroborate; ammonium formate; sodium hydride; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; ethanol; dichloromethane; Isopropyl acetate; water; mineral oil;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / dichloromethane / -6 - 20 °C / Inert atmosphere
2.1: sodium hydride / 1-methyl-pyrrolidin-2-one; mineral oil / 1.5 h / 5 - 20 °C / Inert atmosphere
2.2: 3 h / 68 °C
3.1: ammonium formate / palladium 10% on activated carbon / ethanol / 15.5 h / 60 - 71 °C / Inert atmosphere
4.1: water; Isopropyl acetate / 60 °C
With
ammonium formate; sodium hydride; triethylamine;
palladium 10% on activated carbon;
In
1-methyl-pyrrolidin-2-one; ethanol; dichloromethane; Isopropyl acetate; water; mineral oil;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: diethyl ether / 8 - 20 °C / Inert atmosphere
2.1: N,N-dimethyl-formamide / 4.5 h / 18 - 95 °C / Inert atmosphere
3.1: sodium tetrahydroborate; methanol / tetrahydrofuran / -4 - 27 °C / Inert atmosphere
4.1: triethylamine / dichloromethane / -6 - 20 °C / Inert atmosphere
5.1: sodium hydride / 1-methyl-pyrrolidin-2-one; mineral oil / 1.5 h / 5 - 20 °C / Inert atmosphere
5.2: 3 h / 68 °C
6.1: ammonium formate / palladium 10% on activated carbon / ethanol / 15.5 h / 60 - 71 °C / Inert atmosphere
7.1: water; Isopropyl acetate / 60 °C
With
methanol; sodium tetrahydroborate; ammonium formate; sodium hydride; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; diethyl ether; ethanol; dichloromethane; Isopropyl acetate; water; N,N-dimethyl-formamide; mineral oil;