C₆⁽¹³⁾C₉H₁₃I₂⁽¹⁵⁾NO₄

Base Information

Chemical Name:C₆⁽¹³⁾C₉H₁₃I₂⁽¹⁵⁾NO₄
CAS No.:1431868-08-4
Molecular Formula:C₁₅H₁₃I₂NO₄
Molecular Weight:534.976
Hs Code.:

C<sub>6</sub><sup>(13)</sup>C<sub>9</sub>H<sub>13</sub>I<sub>2</sub><sup>(15)</sup>NO<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆⁽¹³⁾C₉H₁₃I₂⁽¹⁵⁾NO₄

Chemical Property:

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Technology Process of C₆⁽¹³⁾C₉H₁₃I₂⁽¹⁵⁾NO₄

There total 7 articles about C₆⁽¹³⁾C₉H₁₃I₂⁽¹⁵⁾NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁⁽¹³⁾C₉H₂₁I₂⁽¹⁵⁾NO₆

: 1431868-08-4
C₆⁽¹³⁾C₉H₁₃I₂⁽¹⁵⁾NO₄

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; Inert atmosphere;
DOI:10.1080/00397911.2011.639005

Reference yield:

: 1431868-03-9
C₆⁽¹³⁾C₉H₂₁⁽¹⁵⁾NO₅

: 1431868-08-4
C₆⁽¹³⁾C₉H₁₃I₂⁽¹⁵⁾NO₄

Guidance literature:: Multi-step reaction with 5 steps

1: N-iodo-succinimide / dichloromethane / 0.67 h / 0 °C

2: N-ethyl-N,N-diisopropylamine; pyridine; copper diacetate / dichloromethane / 48 h / 20 °C / Molecular sieve

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 0 - 20 °C

4: lithium hydroxide / water; methanol / 1.5 h / 4 °C

5: hydrogenchloride / 1,4-dioxane / 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; N-iodo-succinimide; tetrabutyl ammonium fluoride; copper diacetate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water;
DOI:10.1080/00397911.2011.639005

Reference yield:

: C₂₁⁽¹³⁾C₉H₄₃I₂⁽¹⁵⁾NO₆Si

: 1431868-08-4
C₆⁽¹³⁾C₉H₁₃I₂⁽¹⁵⁾NO₄

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 0 - 20 °C

2: lithium hydroxide / water; methanol / 1.5 h / 4 °C

3: hydrogenchloride / 1,4-dioxane / 20 °C / Inert atmosphere

With hydrogenchloride; tetrabutyl ammonium fluoride; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; water;
DOI:10.1080/00397911.2011.639005