C₃₃H₄₄O₅

Base Information

Chemical Name:C₃₃H₄₄O₅
CAS No.:1376709-22-6
Molecular Formula:C₃₃H₄₄O₅
Molecular Weight:520.709
Hs Code.:

C<sub>33</sub>H<sub>44</sub>O<sub>5</sub>

Synonyms:

Suppliers and Price of C₃₃H₄₄O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₄₄O₅

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₃₃H₄₄O₅

There total 25 articles about C₃₃H₄₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₄₆O₆

: 1376709-22-6
C₃₃H₄₄O₅

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; at 20 ℃;
DOI:10.1039/c3ob40120k

Reference yield:

: 20038-12-4
4-bromo-2-methylbut-1-ene

: 1376709-22-6
C₃₃H₄₄O₅

Guidance literature:: Multi-step reaction with 11 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

2.1: lithium hydroxide / water

3.1: copper(l) cyanide / diethyl ether

4.1: diisobutylaluminium hydride / tetrahydrofuran

5.1: tin(II) trifluoromethanesulfonate; 1-ethyl-piperidine / dichloromethane / 4 h / -50 °C

5.2: -78 °C

6.1: 2,6-dimethylpyridine / dichloromethane

7.1: cerium(III) chloride / tetrahydrofuran / -78 - 20 °C

7.2: silica gel

8.1: N-Bromosuccinimide; methyloxirane / tetrahydrofuran / 20 °C

8.2: 12 h / 20 °C

9.1: samarium diiodide / tetrahydrofuran / 0 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

11.1: pyridinium p-toluenesulfonate / dichloromethane / 20 °C

With 1-ethyl-piperidine; 2,6-dimethylpyridine; N-Bromosuccinimide; tin(II) trifluoromethanesulfonate; samarium diiodide; cerium(III) chloride; tetrabutyl ammonium fluoride; copper(l) cyanide; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; methyloxirane; lithium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; water; 9.1: |Barbier Coupling Reaction;
DOI:10.1039/c3ob40120k

Reference yield:

: 110995-23-8
ethyl 7-methyl-3-oxo-7-octenate

: 1376709-22-6
C₃₃H₄₄O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: lithium hydroxide / water

2.1: copper(l) cyanide / diethyl ether

3.1: diisobutylaluminium hydride / tetrahydrofuran

4.1: tin(II) trifluoromethanesulfonate; 1-ethyl-piperidine / dichloromethane / 4 h / -50 °C

4.2: -78 °C

5.1: 2,6-dimethylpyridine / dichloromethane

6.1: cerium(III) chloride / tetrahydrofuran / -78 - 20 °C

6.2: silica gel

7.1: N-Bromosuccinimide; methyloxirane / tetrahydrofuran / 20 °C

7.2: 12 h / 20 °C

8.1: samarium diiodide / tetrahydrofuran / 0 °C

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

10.1: pyridinium p-toluenesulfonate / dichloromethane / 20 °C

With 1-ethyl-piperidine; 2,6-dimethylpyridine; N-Bromosuccinimide; tin(II) trifluoromethanesulfonate; samarium diiodide; cerium(III) chloride; tetrabutyl ammonium fluoride; copper(l) cyanide; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; methyloxirane; lithium hydroxide; In tetrahydrofuran; diethyl ether; dichloromethane; water; 8.1: |Barbier Coupling Reaction;
DOI:10.1039/c3ob40120k