N-α-hydrocinnamoyl-L-norleucyl)-4(S)-amino-3(S)-hydroxy-6-methylheptanoyl>-L-isoleucyl>-2-pyridylmethylamine

Base Information

Chemical Name:N-α-hydrocinnamoyl-L-norleucyl)-4(S)-amino-3(S)-hydroxy-6-methylheptanoyl>-L-isoleucyl>-2-pyridylmethylamine
CAS No.:114155-88-3
Molecular Formula:C₃₅H₅₃N₅O₅
Molecular Weight:623.836
Hs Code.:

N-<N-<N-(N<sup>α</sup>-hydrocinnamoyl-L-norleucyl)-4(S)-amino-3(S)-hydroxy-6-methylheptanoyl>-L-isoleucyl>-2-pyridylmethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-α-hydrocinnamoyl-L-norleucyl)-4(S)-amino-3(S)-hydroxy-6-methylheptanoyl>-L-isoleucyl>-2-pyridylmethylamine

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Technology Process of N-α-hydrocinnamoyl-L-norleucyl)-4(S)-amino-3(S)-hydroxy-6-methylheptanoyl>-L-isoleucyl>-2-pyridylmethylamine

There total 4 articles about N-α-hydrocinnamoyl-L-norleucyl)-4(S)-amino-3(S)-hydroxy-6-methylheptanoyl>-L-isoleucyl>-2-pyridylmethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58521-49-6
(3S,4S)-4-(tert-butoxycarbonylamino)-3-hydroxy-6-methylheptanoic acid

: 114155-88-3
N-α-hydrocinnamoyl-L-norleucyl)-4(S)-amino-3(S)-hydroxy-6-methylheptanoyl>-L-isoleucyl>-2-pyridylmethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / diisopropylethylamine, diethyl phosphorocyanidate / CH₂Cl₂ / 6 h

2: 1.) HCl, 2.) diisopropylethylamine, diethyl phosphorocyanidate / 1) ether, 15 min; 2) CH₂Cl₂, overnight

3: 1.) trifluoroacetic acid, 2.) diisopropylethylamine, diethyl phosphorocyanidate / 1) CH₂Cl₂, 40 min, room temperature; 2) CH₂Cl₂, overnight

With hydrogenchloride; diethyl cyanophosphonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm00402a021

Reference yield:

: 97920-16-6
N-L-isoleucyl-2-pyridylmethylamine

: 114155-88-3
N-α-hydrocinnamoyl-L-norleucyl)-4(S)-amino-3(S)-hydroxy-6-methylheptanoyl>-L-isoleucyl>-2-pyridylmethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / diisopropylethylamine, diethyl phosphorocyanidate / CH₂Cl₂ / 6 h

2: 1.) HCl, 2.) diisopropylethylamine, diethyl phosphorocyanidate / 1) ether, 15 min; 2) CH₂Cl₂, overnight

3: 1.) trifluoroacetic acid, 2.) diisopropylethylamine, diethyl phosphorocyanidate / 1) CH₂Cl₂, 40 min, room temperature; 2) CH₂Cl₂, overnight

With hydrogenchloride; diethyl cyanophosphonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm00402a021

Reference yield:

: 103372-24-3
N-α-<4(S)-<(tert-butyloxycarbonyl)amino>-3(S)-hydroxy-6-methylheptanoyl>-L-isoleucyl>-2-pyridylmethylamine

: 114155-88-3
N-α-hydrocinnamoyl-L-norleucyl)-4(S)-amino-3(S)-hydroxy-6-methylheptanoyl>-L-isoleucyl>-2-pyridylmethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) HCl, 2.) diisopropylethylamine, diethyl phosphorocyanidate / 1) ether, 15 min; 2) CH₂Cl₂, overnight

2: 1.) trifluoroacetic acid, 2.) diisopropylethylamine, diethyl phosphorocyanidate / 1) CH₂Cl₂, 40 min, room temperature; 2) CH₂Cl₂, overnight

With hydrogenchloride; diethyl cyanophosphonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
DOI:10.1021/jm00402a021