(rac.-1R,2S,3S,1'S)-N--1,2-epoxy-3-methyl-4,4-dioxyethylene-cyclohexane-1-carbonamide

Base Information

Chemical Name:(rac.-1R,2S,3S,1'S)-N--1,2-epoxy-3-methyl-4,4-dioxyethylene-cyclohexane-1-carbonamide
CAS No.:94168-92-0
Molecular Formula:C₂₁H₂₅NO₇
Molecular Weight:403.432
Hs Code.:

(rac.-1R,2S,3S,1'S)-N-<benzoyl(ethoxycarbonyl)methyl>-1,2-epoxy-3-methyl-4,4-dioxyethylene-cyclohexane-1-carbonamide

Synonyms:

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Chemical Property of (rac.-1R,2S,3S,1'S)-N--1,2-epoxy-3-methyl-4,4-dioxyethylene-cyclohexane-1-carbonamide

Chemical Property:

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Technology Process of (rac.-1R,2S,3S,1'S)-N--1,2-epoxy-3-methyl-4,4-dioxyethylene-cyclohexane-1-carbonamide

There total 8 articles about (rac.-1R,2S,3S,1'S)-N--1,2-epoxy-3-methyl-4,4-dioxyethylene-cyclohexane-1-carbonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94169-08-1
methyl-3-methyl-4-oxy-2-cyclohexene-1-carboxylate

: 94168-92-0,94234-12-5
(rac.-1R,2S,3S,1'R)-N--1,2-epoxy-3-methyl-4,4-dioxyethylene-cyclohexane-1-carbonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / p-TosOH / benzene / 20 h / Heating

2: 26 percent / m CPBA / benzene / 16 h / Heating

3: 1.) Na, 2.) pyridine / 1.) EtOH, H₂O, RT, 16 h; 2.) THF, -20 deg C up to RT

4: Et₃N / tetrahydrofuran

With pyridine; sodium; toluene-4-sulfonic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; benzene;
DOI:10.1016/0040-4020(84)85020-6

Reference yield:

: 94169-08-1
methyl-3-methyl-4-oxy-2-cyclohexene-1-carboxylate

: 94168-92-0,94234-12-5
(rac.-1R,2S,3S,1'S)-N--1,2-epoxy-3-methyl-4,4-dioxyethylene-cyclohexane-1-carbonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / p-TosOH / benzene / 20 h / Heating

2: 26 percent / m CPBA / benzene / 16 h / Heating

3: 1.) Na, 2.) pyridine / 1.) EtOH, H₂O, RT, 16 h; 2.) THF, -20 deg C up to RT

4: Et₃N / tetrahydrofuran

With pyridine; sodium; toluene-4-sulfonic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; benzene;
DOI:10.1016/0040-4020(84)85020-6

Reference yield:

: 94169-09-2
methyl 3-methyl-4,4-dioxyethylene-1-cyclohexene-1-carboxylate

: 94168-92-0,94234-12-5
(rac.-1R,2S,3S,1'R)-N--1,2-epoxy-3-methyl-4,4-dioxyethylene-cyclohexane-1-carbonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 26 percent / m CPBA / benzene / 16 h / Heating

2: 1.) Na, 2.) pyridine / 1.) EtOH, H₂O, RT, 16 h; 2.) THF, -20 deg C up to RT

3: Et₃N / tetrahydrofuran

With pyridine; sodium; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; benzene;
DOI:10.1016/0040-4020(84)85020-6