9--9,10-dihydro-10-methylacridine

Base Information

Chemical Name:9--9,10-dihydro-10-methylacridine
CAS No.:68066-94-4
Molecular Formula:C₂₇H₁₉Cl₂N
Molecular Weight:428.361
Hs Code.:

9-<bis(p-chlorophenyl)-methylene>-9,10-dihydro-10-methylacridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9--9,10-dihydro-10-methylacridine

Chemical Property:

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Technology Process of 9--9,10-dihydro-10-methylacridine

There total 3 articles about 9--9,10-dihydro-10-methylacridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 9-methyl-9-azonianthracene methyl sulfate

: 68066-94-4
9--9,10-dihydro-10-methylacridine

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / NaI / acetonitrile / 2 h

2: 1) BuLi / 1) hexane, THF, -78 deg C, 2) THF, 10 min; reflux, 45 min

With n-butyllithium; sodium iodide; In acetonitrile;
DOI:10.1007/BF00809369

Reference yield:

: 65674-22-8
10-dimethoxyphosphinyl-9-methyl-9,10-dihydro-9-azaanthracene

: 90-98-2
4,4'-Dichlorobenzophenone

: 68066-94-4
9--9,10-dihydro-10-methylacridine

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1) hexane, THF, -78 deg C, 2) THF, 10 min; reflux, 45 min;
DOI:10.1007/BF00809369