BOC-THR(FMOC-GLY)-OH

Base Information

• Chemical Name: BOC-THR(FMOC-GLY)-OH
• CAS No.: 944283-25-4
• Molecular Formula: C₂₆H₃₀N₂O₈
• Molecular Weight: 498.533
• Mol file: 944283-25-4.mol

Synonyms:N-[(1,1-Dimethylethoxy)carbonyl]-O-[N-[(9H-fluoren-9-ylmethoxy)carbonyl]glycyl]-L-threonine;L-Threonine, N-[(1,1-dimethylethoxy)carbonyl]-O-[N-[(9H-fluoren-9-ylmethoxy)carbonyl]glycyl]-;

Chemical Property of BOC-THR(FMOC-GLY)-OH

Chemical Property:

• PSA: 140.26000
• LogP: 4.21650

Purity/Quality:

99% ^*data from raw suppliers

Boc-Thr(Gly-Fmoc)-OH,≥97%(HPLC) ≥97%(HPLC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of BOC-THR(FMOC-GLY)-OH

There total 3 articles about BOC-THR(FMOC-GLY)-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Boc-Thr(Fmoc-Gly)-OBzl → Boc-Thr(Fmoc-Gly)-OH (944283-25-4)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate;

DOI:10.1039/b702284k

Reference yield:

N-(fluoren-9-ylmethoxycarbonyl)glycine (29022-11-5) → Boc-Thr(Fmoc-Gly)-OH (944283-25-4)

Guidance literature:

Multi-step reaction with 2 steps

1: N-ethyl-N'-(3-dimethylaminopropyl)-carbodiimide*HCl; N,N-dimethylaminopyridine / CHCl₃ / 0 - 20 °C

2: H₂ / Pd/C / ethyl acetate

With dmap; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In chloroform; ethyl acetate;

DOI:10.1039/b702284k

Reference yield:

N-(tert-butyloxycarbonyl)-threonine benzyl ester (140422-54-4,33662-26-9) → Boc-Thr(Fmoc-Gly)-OH (944283-25-4)

Guidance literature:

Multi-step reaction with 2 steps

1: N-ethyl-N'-(3-dimethylaminopropyl)-carbodiimide*HCl; N,N-dimethylaminopyridine / CHCl₃ / 0 - 20 °C

2: H₂ / Pd/C / ethyl acetate

With dmap; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In chloroform; ethyl acetate;

DOI:10.1039/b702284k

upstream raw materials:

N-(fluoren-9-ylmethoxycarbonyl)glycine

N-(tert-butyloxycarbonyl)-threonine benzyl ester

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