10-Phenyl-1-decanol

Base Information

• Chemical Name: 10-Phenyl-1-decanol
• CAS No.: 62607-69-6
• Molecular Formula: C16H26O
• Molecular Weight: 234.382
• Hs Code.: 2906299090
• Mol file: 62607-69-6.mol

Synonyms:10-PHENYL-1-DECANOL;10-PHENYL-N-DECANOL;10-PHENYLDECANOL;10-Phenyl-1-decanol,96%;10-Phenyldecan-1-ol

Chemical Property of 10-Phenyl-1-decanol

Chemical Property:

• Appearance/Colour: white solid
• Vapor Pressure: 2.56E-05mmHg at 25°C
• Melting Point: 35-37°C
• Refractive Index: 1.502
• Boiling Point: 344.2 °C at 760 mmHg
• PKA: 15.20±0.10(Predicted)
• Flash Point: 126.5 °C
• PSA: 20.23000
• Density: 0.93 g/cm³
• LogP: 4.34220

Purity/Quality:

99% ^*data from raw suppliers

10-Phenyl-1-decanol, 96% ^*data from reagent suppliers

Safty Information:

• Safety Statements: S24/25:Avoid contact with skin and eyes.

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 10-Phenyl-1-decanol

There total 6 articles about 10-Phenyl-1-decanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(10-Phenyl-decyloxy)-tetrahydro-pyran → 10-phenyl-1-decanol (62607-69-6)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; for 8h; Yield given; Ambient temperature;

DOI:10.1246/bcsj.64.1054

Reference yield:

phenylmagnesium bromide → 10-phenyl-1-decanol (62607-69-6)

Guidance literature:

Multi-step reaction with 2 steps

1: CuCl / tetrahydrofuran / 5 h / Heating

2: p-TsOH / methanol / 8 h / Ambient temperature

With toluene-4-sulfonic acid; copper(l) chloride; In tetrahydrofuran; methanol;

DOI:10.1246/bcsj.64.1054

Reference yield:

10-tetrahydropyranyloxydecanol (43047-93-4) → 10-phenyl-1-decanol (62607-69-6)

Guidance literature:

Multi-step reaction with 4 steps

1: (COCl)2, DMSO, Et₃N / CH₂Cl₂

2: diethyl ether

3: Et₃SiH, CF₃CO₂H

4: NaOH / methanol

With triethylsilane; sodium hydroxide; oxalyl dichloride; dimethyl sulfoxide; triethylamine; trifluoroacetic acid; In methanol; diethyl ether; dichloromethane;

DOI:10.1039/c39860001234

upstream raw materials:

10-tetrahydropyranyloxydecanol

1,10-Decanediol

10-(tetrahydropyran-2'-yloxy)decanal

1-Phenyl-10-(tetrahydro-pyran-2-yloxy)-decan-1-ol

Downstream raw materials:

10-phenyl-decanal

n-nonylbenzene

Refernces

• 1、 Furukawa, Yoshiaki,Yamagiwa, Yoshiro,Kamikawa, Tadao. "Synthesis of 3-(ω-Phenylalkyl)catechols, Phenolic Lipids found in Sap of the Burmese Lac Tree, via Directed Metallation". . p. 1234 - 1235. Retrieved 2007/10/02.