tert-butyl 2-(5-methylfuran-2-yl)ethylcarbamate

Base Information

Chemical Name:tert-butyl 2-(5-methylfuran-2-yl)ethylcarbamate
CAS No.:537041-67-1
Molecular Formula:C12H19NO3
Molecular Weight:225.28
Hs Code.:
Mol file:537041-67-1.mol

Synonyms:N-Boc-2-Aminoethyl-5-methylfuran;tert-butyl 2-(5-methylfuran-2-yl)ethylcarbamate;Carbamic acid, [2-(5-methyl-2-furanyl)ethyl]-, 1,1-dimethylethyl ester (9CI)

Suppliers and Price of tert-butyl 2-(5-methylfuran-2-yl)ethylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl(2-(5-methylfuran-2-yl)ethyl)carbamate 95+%
1g
$ 402.00

Chemenu
tert-butyl(2-(5-methylfuran-2-yl)ethyl)carbamate 95%
1g
$ 380.00

Alichem
tert-Butyl(2-(5-methylfuran-2-yl)ethyl)carbamate
1g
$ 328.00

Total 9 raw suppliers

Chemical Property of tert-butyl 2-(5-methylfuran-2-yl)ethylcarbamate

Chemical Property:

PSA：54.96000
LogP:2.85960
Storage Temp.:2-8°C

Purity/Quality:

99% ^*data from raw suppliers

tert-Butyl(2-(5-methylfuran-2-yl)ethyl)carbamate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tert-butyl 2-(5-methylfuran-2-yl)ethylcarbamate

There total 2 articles about tert-butyl 2-(5-methylfuran-2-yl)ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 30796-85-1
β-(5-methyl-2-furanyl)ethanamine

: 24424-99-5
di-tert-butyl dicarbonate

: 537041-67-1
[2-(5-methyl-furan-2-yl)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 620-02-0
5-Methylfurfural

: 537041-67-1
[2-(5-methyl-furan-2-yl)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaOH / methanol; H₂O / -10 °C

1.2: lithium aluminium hydride / tetrahydrofuran / 12 h / Heating

2.1: 92 percent / DMAP / CH₂Cl₂ / 2 h / 20 °C

With dmap; sodium hydroxide; In methanol; dichloromethane; water; 1.1: Henry reaction;