Technology Process of C21H16O
There total 3 articles about C21H16O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride;
In
benzene;
for 48h;
Heating;
DOI:10.1021/jo00282a022
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 20 percent / isoamyl nitrite / 1,2-dimethoxy-ethane / 5 h / Heating
2: 80 percent / tributyltin hydride (TBH), azobisisobutyronitrile (AIBN) / benzene / 48 h / Heating
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; isopentyl nitrite;
In
1,2-dimethoxyethane; benzene;
DOI:10.1021/jo00282a022
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) n-BuLi / 1.) ether/hexane, reflux, 4 h, 2.) reflux, 16 h
2: 20 percent / isoamyl nitrite / 1,2-dimethoxy-ethane / 5 h / Heating
3: 80 percent / tributyltin hydride (TBH), azobisisobutyronitrile (AIBN) / benzene / 48 h / Heating
With
n-butyllithium; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; isopentyl nitrite;
In
1,2-dimethoxyethane; benzene;
DOI:10.1021/jo00282a022