Ta(NNCHPh)(O-2,6-C₆H₃-i-Pr₂)3(THF)

Base Information

Chemical Name:Ta(NNCHPh)(O-2,6-C₆H₃-i-Pr₂)3(THF)
CAS No.:114198-82-2
Molecular Formula:C₄H₈O*C₇H₆N₂*3C₁₂H₁₇O*Ta
Molecular Weight:902.992
Hs Code.:

Ta(NNCHPh)(O-2,6-C<sub>6</sub>H<sub>3</sub>-i-Pr<sub>2</sub>)3(THF)

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Chemical Property of Ta(NNCHPh)(O-2,6-C₆H₃-i-Pr₂)3(THF)

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Technology Process of Ta(NNCHPh)(O-2,6-C₆H₃-i-Pr₂)3(THF)

There total 1 articles about Ta(NNCHPh)(O-2,6-C₆H₃-i-Pr₂)3(THF) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 106034-24-6
Ta(CH-t-Bu)(O-2,6-C₆H₃-i-Pr₂)3(THF)

: 588-68-1,28867-76-7,65997-87-7,65997-88-8
benzaldehyde azine

: 114198-82-2
Ta(NNCHPh)(O-2,6-C₆H₃-i-Pr₂)3(THF)

Guidance literature:: In diethyl ether; byproducts: PhCH=CHCMe3; A soln. of benzaldehyde azine in ether was added to a soln. of Ta(CH-t-Bu)(DIPP)3(THF) in a mixt. of ether and THF at -30°C. The soln. was stirred at 25°C; there was little color change. PhCH=CHCMe3 is a further product.; After 30 min the soln. was filtered, and the solvent was removed in vacuo. The resulting yellow oil was dissolved in pentane, and the soln. was cooled to -30°C to yield crystals. Elem.anal.;