((3-(4-(((2-methoxybenzoyl)(6-(4-(benzyloxy)phenoxy)-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester

Base Information

• Chemical Name: ((3-(4-(((2-methoxybenzoyl)(6-(4-(benzyloxy)phenoxy)-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester
• CAS No.: 754992-80-8
• Molecular Formula: C₄₉H₅₃N₅O₉S
• Molecular Weight: 888.054

Synonyms:

Chemical Property of ((3-(4-(((2-methoxybenzoyl)(6-(4-(benzyloxy)phenoxy)-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester

Chemical Property:

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Technology Process of ((3-(4-(((2-methoxybenzoyl)(6-(4-(benzyloxy)phenoxy)-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester

There total 2 articles about ((3-(4-(((2-methoxybenzoyl)(6-(4-(benzyloxy)phenoxy)-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(6-(4-benzyloxyphenoxy)benzothiazol-2-yl)-N-(4-(3-(1,3-dihydro-1,3-dioxoisoindol-2-yl)propoxy)benzyl)-2-methoxybenzamide (754992-77-3) → ((3-(4-(((2-methoxybenzoyl)(6-(4-(benzyloxy)phenoxy)-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester (754992-80-8)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 68 °C

2: 0.123 g / CH₂Cl₂ / 20 °C

With hydrazine hydrate; In ethanol; dichloromethane;

DOI:10.1016/j.bmc.2004.05.040

Reference yield:

N,N'-bis( tert-butoxycarbonyl)-1H-pyrazole-1-carboxamidine (152120-54-2,862686-58-6,1143572-00-2) + N-[4-(3-amino-propoxy)-benzyl]-N-[6-(4-benzyloxy-phenoxy)-benzothiazol-2-yl]-2-methoxy-benzamide (754992-84-2) → ((3-(4-(((2-methoxybenzoyl)(6-(4-(benzyloxy)phenoxy)-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester (754992-80-8)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1016/j.bmc.2004.05.040

Reference yield: 70.0%

((3-(4-(((2-methoxybenzoyl)(6-(4-(benzyloxy)phenoxy)-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester (754992-80-8) → N-[4-(3-guanidino-propoxy)-benzyl]-N-[6-(4-hydroxy-phenoxy)-benzothiazol-2-yl]-2-methoxy-benzamide

Guidance literature:

With methyl-phenyl-thioether; trifluoroacetic acid; for 6h;

DOI:10.1016/j.bmc.2004.05.040

upstream raw materials:

N,N'-bis( tert-butoxycarbonyl)-1H-pyrazole-1-carboxamidine

N-[4-(3-amino-propoxy)-benzyl]-N-[6-(4-benzyloxy-phenoxy)-benzothiazol-2-yl]-2-methoxy-benzamide

N-(6-(4-benzyloxyphenoxy)benzothiazol-2-yl)-N-(4-(3-(1,3-dihydro-1,3-dioxoisoindol-2-yl)propoxy)benzyl)-2-methoxybenzamide

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