C₉H₁₀N₃⁽¹⁺⁾*CH₃O₄S^(1-)

Base Information

• Chemical Name: C₉H₁₀N₃⁽¹⁺⁾*CH₃O₄S^(1-)
• CAS No.: 120317-71-7
• Molecular Formula: CH₃O₄S*C₉H₁₀N₃
• Molecular Weight: 271.297
• Mol file: 120317-71-7.mol

Synonyms:

Chemical Property of C₉H₁₀N₃⁽¹⁺⁾*CH₃O₄S^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₉H₁₀N₃⁽¹⁺⁾*CH₃O₄S^(1-)

There total 2 articles about C₉H₁₀N₃⁽¹⁺⁾*CH₃O₄S^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

aniline (62-53-3) → C9H10N3(1+)*CH3O4S(1-) (120317-71-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 50 percent / (NH₄)2SO₄ / 3 h / 180 °C

2: acetonitrile / 4 h / Heating

With ammonium sulfate; In acetonitrile;

Reference yield:

1-phenyl-1,3,4-triazole (16227-12-6) + dimethyl sulfate (77-78-1) → C9H10N3(1+)*CH3O4S(1-) (120317-71-7)

Guidance literature:

In acetonitrile; for 4h; Yield given; Heating;

Reference yield:

4-(dimethylamino)benzenediazonium tetrafluoroborate (24564-52-1) + C9H10N3(1+)*CH3O4S(1-) (120317-71-7) → C17H19N6(1+)*BF4(1-)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; triethylamine; for 0.0833333h; Yield given;

upstream raw materials:

1-phenyl-1,3,4-triazole

dimethyl sulfate

aniline

Refernces