[1,2-bis(dimethylphosphino)ethane](η-cyclopentadienyl)(diphenylacetylene)molybdenum hexafluorophosphate

Base Information

• Chemical Name: [1,2-bis(dimethylphosphino)ethane](η-cyclopentadienyl)(diphenylacetylene)molybdenum hexafluorophosphate
• CAS No.: 77187-15-6
• Molecular Formula: C₂₅H₃₁MoP₂*F₆P
• Molecular Weight: 634.373
• Mol file: 77187-15-6.mol

Synonyms:

Chemical Property of [1,2-bis(dimethylphosphino)ethane](η-cyclopentadienyl)(diphenylacetylene)molybdenum hexafluorophosphate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [1,2-bis(dimethylphosphino)ethane](η-cyclopentadienyl)(diphenylacetylene)molybdenum hexafluorophosphate

There total 1 articles about [1,2-bis(dimethylphosphino)ethane](η-cyclopentadienyl)(diphenylacetylene)molybdenum hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

[1,2-bis(dimethylphosphino)ethane](η-cyclopentadienyl)tetrahydridomolybdenum hexafluorophosphate (77187-13-4) + diphenyl acetylene (501-65-5) → [1,2-bis(dimethylphosphino)ethane](η-cyclopentadienyl)(diphenylacetylene)molybdenum hexafluorophosphate (77187-15-6)

Guidance literature:

In acetonitrile; in vac., or under an inert atm., warmed to 70°C for 5 min; concd. in vac., addn. of Et2O, ppt. sepd., washing with ether, dried invac., elem. anal.;

DOI:10.1039/DT9810000353

upstream raw materials:

[1,2-bis(dimethylphosphino)ethane](η-cyclopentadienyl)tetrahydridomolybdenum hexafluorophosphate

diphenyl acetylene