7,7'-Dibromo-3,3',5,5'-tetramethyl-1,1'-biadamantane

Base Information

• Chemical Name: 7,7'-Dibromo-3,3',5,5'-tetramethyl-1,1'-biadamantane
• CAS No.: 63263-14-9
• Molecular Formula: C24H36Br2
• Molecular Weight: 484.35064
• Mol file: 63263-14-9.mol

Synonyms:3,3'-Dibromo-5,5',7,7'-tetramethyl-1,1'-biadamantane;7,7'-Dibromo-3,3',5,5'-tetramethyl-1,1'-biadamantane

Chemical Property of 7,7'-Dibromo-3,3',5,5'-tetramethyl-1,1'-biadamantane

Chemical Property:

• PSA: 0.00000
• Density: 1.516
• LogP: 8.01460

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 7,7'-Dibromo-3,3',5,5'-tetramethyl-1,1'-biadamantane

There total 2 articles about 7,7'-Dibromo-3,3',5,5'-tetramethyl-1,1'-biadamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3',5,5'-tetramethyl-1,1'-biadamantane (58156-57-3) → 3,3'-dibromo-5,5',7,7'-tetramethyl-1,1'-biadamantane (63263-14-9)

Guidance literature:

With bromine; In diethyl ether;

DOI:10.1039/P29770000505

Reference yield:

3,5-dimethyl-1-bromoadamantane (941-37-7) → 3,3'-dibromo-5,5',7,7'-tetramethyl-1,1'-biadamantane (63263-14-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Mg, AgBr / diethyl ether

2: Br₂ / diethyl ether

With silver(I) bromide; bromine; magnesium; In diethyl ether;

DOI:10.1039/P29770000505

upstream raw materials:

3,3',5,5'-tetramethyl-1,1'-biadamantane

3,5-dimethyl-1-bromoadamantane