bis(acetophenone benzoylhydrazone)nickel(II) chloride monohydrate

Base Information

• Chemical Name: bis(acetophenone benzoylhydrazone)nickel(II) chloride monohydrate
• CAS No.: 385819-22-7
• Molecular Formula: C₃₀H₂₈Cl₂N₄NiO₂*H₂O
• Molecular Weight: 624.189
• Mol file: 385819-22-7.mol

Synonyms:

Chemical Property of bis(acetophenone benzoylhydrazone)nickel(II) chloride monohydrate

Chemical Property:

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Technology Process of bis(acetophenone benzoylhydrazone)nickel(II) chloride monohydrate

There total 1 articles about bis(acetophenone benzoylhydrazone)nickel(II) chloride monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

nickel(II) dichloride hydrate + acetophenone benzoyl hydrazone (14850-96-5) → bis(acetophenone benzoylhydrazone)nickel(II) chloride monohydrate (385819-22-7)

Guidance literature:

In ethanol; water; byproducts: H2O; 0.5 equiv. of metal chloride in 1:1 EtOH:H2O (v/v) was added to a hot EtOH soln. of hydrazone-compd., heating on water bath for 1 h; ppt. was filtered off, washed with distd. water and EtOH, finally with Et2O, dried over anhyd. CaCl2 in a desiccator in vac., elem. anal.;

DOI:10.1081/SIM-100107204

upstream raw materials:

acetophenone benzoyl hydrazone