[4-Methoxy-3-(2-nitro-benzyloxy)-phenyl]-acetic acid methyl ester

Base Information

Chemical Name:[4-Methoxy-3-(2-nitro-benzyloxy)-phenyl]-acetic acid methyl ester
CAS No.:129249-78-1
Molecular Formula:C₁₇H₁₇NO₆
Molecular Weight:331.325
Hs Code.:

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Chemical Property of [4-Methoxy-3-(2-nitro-benzyloxy)-phenyl]-acetic acid methyl ester

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Technology Process of [4-Methoxy-3-(2-nitro-benzyloxy)-phenyl]-acetic acid methyl ester

There total 6 articles about [4-Methoxy-3-(2-nitro-benzyloxy)-phenyl]-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88-72-2
1-methyl-2-nitrobenzene

: 129249-78-1
[4-Methoxy-3-(2-nitro-benzyloxy)-phenyl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 77 percent / N-bromosuccinimide / CCl₄ / 3 h / Heating; Irradiation

2: 86.6 percent / K₂CO₃ / methanol / 5 h / Heating

3: 85 percent / SOCl₂, N,N-dimethylaniline / benzene / 1 h / Heating

4: 81 percent / KI / acetone / 20 h / Heating

5: 82 percent / aq. H₂SO₄ / acetic acid / 1 h / Heating

6: 2 g / diethyl ether; methanol

With N-Bromosuccinimide; thionyl chloride; sulfuric acid; potassium carbonate; N,N-dimethyl-aniline; potassium iodide; In methanol; tetrachloromethane; diethyl ether; acetic acid; acetone; benzene;

Reference yield:

: 3958-60-9
2-nitrophenylmethyl bromide

: 129249-78-1
[4-Methoxy-3-(2-nitro-benzyloxy)-phenyl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 86.6 percent / K₂CO₃ / methanol / 5 h / Heating

2: 85 percent / SOCl₂, N,N-dimethylaniline / benzene / 1 h / Heating

3: 81 percent / KI / acetone / 20 h / Heating

4: 82 percent / aq. H₂SO₄ / acetic acid / 1 h / Heating

5: 2 g / diethyl ether; methanol

With thionyl chloride; sulfuric acid; potassium carbonate; N,N-dimethyl-aniline; potassium iodide; In methanol; diethyl ether; acetic acid; acetone; benzene;

Reference yield:

: 129271-80-3
4-methoxy-3-(o-nitrobenzyloxy)benzyl alcohol

: 129249-78-1
[4-Methoxy-3-(2-nitro-benzyloxy)-phenyl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / SOCl₂, N,N-dimethylaniline / benzene / 1 h / Heating

2: 81 percent / KI / acetone / 20 h / Heating

3: 82 percent / aq. H₂SO₄ / acetic acid / 1 h / Heating

4: 2 g / diethyl ether; methanol

With thionyl chloride; sulfuric acid; N,N-dimethyl-aniline; potassium iodide; In methanol; diethyl ether; acetic acid; acetone; benzene;