(3,5-(CF₃)2C₆H₃NH_0.5C(CF₃))2CH

Base Information

Chemical Name:(3,5-(CF₃)2C₆H₃NH_0.5C(CF₃))2CH
CAS No.:628301-50-8
Molecular Formula:C₂₁H₈F₁₈N₂
Molecular Weight:630.279
Hs Code.:

(3,5-(CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>NH<sub>0.5</sub>C(CF<sub>3</sub>))2CH

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Chemical Property of (3,5-(CF₃)2C₆H₃NH_0.5C(CF₃))2CH

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Technology Process of (3,5-(CF₃)2C₆H₃NH_0.5C(CF₃))2CH

There total 1 articles about (3,5-(CF₃)2C₆H₃NH_0.5C(CF₃))2CH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1522-20-9,26567-75-9,72036-58-9
acetylacetone

: 328-74-5
3,5-Bis-(trifluoromethyl)aniline

: 628301-50-8
(3,5-(CF₃)2C₆H₃NH_0.5C(CF₃))2CH

Guidance literature:: With titanium tetrachloride; In toluene; Inert atmosphere;
DOI:10.1021/om2006479

Reference yield: 89.0%

: 628301-50-8
(3,5-(CF₃)2C₆H₃NH_0.5C(CF₃))2CH

: 75-05-8,26809-02-9
acetonitrile

: 20667-12-3
silver(l) oxide

: [Ag(CH₃CN)2(3,5-(CF₃)2C₆H₃NC(CF₃))2CH)]2

Guidance literature:: In acetonitrile; byproducts: H2O; other Radiation; (N2); std. Schlenk technique; ligand was added to Ag2O in MeCN; heated under micriwave (400 MW, 1 h); filtered through Celite under N2; evapd. (vac.); washed (pentane); dried(vac., dark);
DOI:10.1021/om2006479