(5Z,10Z,14Z,19Z)-5,15-Bis-(2-{3-[2-(5,5-dimethyl-[1,3]dioxan-2-yl)-phenoxy]-propoxy}-phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-porphyrin

Base Information

Chemical Name:(5Z,10Z,14Z,19Z)-5,15-Bis-(2-{3-[2-(5,5-dimethyl-[1,3]dioxan-2-yl)-phenoxy]-propoxy}-phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-porphyrin
CAS No.:135923-55-6
Molecular Formula:C₇₄H₈₆N₄O₈
Molecular Weight:1159.52
Hs Code.:

(5Z,10Z,14Z,19Z)-5,15-Bis-(2-{3-[2-(5,5-dimethyl-[1,3]dioxan-2-yl)-phenoxy]-propoxy}-phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-porphyrin

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Chemical Property of (5Z,10Z,14Z,19Z)-5,15-Bis-(2-{3-[2-(5,5-dimethyl-[1,3]dioxan-2-yl)-phenoxy]-propoxy}-phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-porphyrin

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Technology Process of (5Z,10Z,14Z,19Z)-5,15-Bis-(2-{3-[2-(5,5-dimethyl-[1,3]dioxan-2-yl)-phenoxy]-propoxy}-phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-porphyrin

There total 7 articles about (5Z,10Z,14Z,19Z)-5,15-Bis-(2-{3-[2-(5,5-dimethyl-[1,3]dioxan-2-yl)-phenoxy]-propoxy}-phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 131161-29-0
2-(3-iodopropoxy)-1-(5,5'-dimethyl-1,3-dioxan-2-yl)benzene

: 135879-45-7
α,α-5,15-bis(2-hydroxyphenyl)ethioporphyrin II

: 135923-55-6
(5Z,10Z,14Z,19Z)-5,15-Bis-(2-{3-[2-(5,5-dimethyl-[1,3]dioxan-2-yl)-phenoxy]-propoxy}-phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-porphyrin

Guidance literature:: With potassium carbonate; In acetone; Heating;
DOI:10.1246/bcsj.64.1213

Reference yield:

: 92415-30-0
bis(3-ethyl-4-methyl-1H-pyrrol-2-yl)methane

: 135923-55-6
(5Z,10Z,14Z,19Z)-5,15-Bis-(2-{3-[2-(5,5-dimethyl-[1,3]dioxan-2-yl)-phenoxy]-propoxy}-phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-porphyrin

Guidance literature:: Multi-step reaction with 3 steps

1: 2) p-chloranil / 1) CCl₃COOH / 1) CH₃CN, 5h, RT, 2) THF, overnight

2: 91 percent / BBr₃ / CH₂Cl₂ / 1) -78 deg C to RT, 2) RT

3: 54 percent / K₂CO₃ / acetone / Heating

With boron tribromide; chloranil; potassium carbonate; trichloroacetic acid; In dichloromethane; acetone;
DOI:10.1246/bcsj.64.1213

Reference yield:

: 53390-00-4
1,4?bis(2?formylphenoxymethyl)benzene (dialdehyde)

: 135923-55-6
(5Z,10Z,14Z,19Z)-5,15-Bis-(2-{3-[2-(5,5-dimethyl-[1,3]dioxan-2-yl)-phenoxy]-propoxy}-phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethyl-porphyrin

Guidance literature:: Multi-step reaction with 3 steps

1: 2) p-chloranil / 1) CCl₃COOH / 1) CH₃CN, 5h, RT, 2) THF, overnight

2: 91 percent / BBr₃ / CH₂Cl₂ / 1) -78 deg C to RT, 2) RT

3: 54 percent / K₂CO₃ / acetone / Heating

With boron tribromide; chloranil; potassium carbonate; trichloroacetic acid; In dichloromethane; acetone;
DOI:10.1246/bcsj.64.1213