P-Bromo-N-(2,4,6-tri-t-butylphenyl)-λ³-iminophosphine

Base Information

Chemical Name:P-Bromo-N-(2,4,6-tri-t-butylphenyl)-λ³-iminophosphine
CAS No.:117688-10-5
Molecular Formula:C₁₈H₂₉BrNP
Molecular Weight:370.313
Hs Code.:

P-Bromo-N-(2,4,6-tri-t-butylphenyl)-λ<sup>3</sup>-iminophosphine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of P-Bromo-N-(2,4,6-tri-t-butylphenyl)-λ³-iminophosphine

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Technology Process of P-Bromo-N-(2,4,6-tri-t-butylphenyl)-λ³-iminophosphine

There total 2 articles about P-Bromo-N-(2,4,6-tri-t-butylphenyl)-λ³-iminophosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 117688-09-2,124775-15-1
P-chloro-N-(2,4,6-tri-tert-butylphenyl)-λ³-iminophosphine

: 117688-10-5,149837-59-2
P-Bromo-N-(2,4,6-tri-t-butylphenyl)-λ³-iminophosphine

Guidance literature:: With trimethylsilyl bromide; In benzene; for 3h;

Reference yield:

: 961-38-6
2,4,6-Tri-tert-butylaniline

: 117688-10-5,149837-59-2
P-Bromo-N-(2,4,6-tri-t-butylphenyl)-λ³-iminophosphine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / PCl₃, Et₃N / pentane / 120 h / Ambient temperature

2: 43 percent / Me₃SiBr / hexane / 3 h / 0 °C

With trimethylsilyl bromide; triethylamine; phosphorus trichloride; In hexane; pentane;