Technology Process of C22H36O3S
There total 12 articles about C22H36O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: diisobutylaluminium hydride / tetrahydrofuran
2: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane
3: sodium hydride / tetrahydrofuran
4: diisobutylaluminium hydride / tetrahydrofuran
5: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane
6: pyridine; tributylphosphine
7: dichloromethane
With
pyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; oxalyl dichloride; diethyl (2S,3S)-tartrate; tributylphosphine; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine;
In
tetrahydrofuran; dichloromethane;
2: Swern oxidation / 3: Horner-Emmons olefination / 5: Katsuki-Sharpless epoxidation;
DOI:10.1016/j.tetlet.2011.10.073
- Guidance literature:
-
Multi-step reaction with 6 steps
1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane
2: sodium hydride / tetrahydrofuran
3: diisobutylaluminium hydride / tetrahydrofuran
4: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane
5: pyridine; tributylphosphine
6: dichloromethane
With
pyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; oxalyl dichloride; diethyl (2S,3S)-tartrate; tributylphosphine; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine;
In
tetrahydrofuran; dichloromethane;
1: Swern oxidation / 2: Horner-Emmons olefination / 4: Katsuki-Sharpless epoxidation;
DOI:10.1016/j.tetlet.2011.10.073