β-Mo2Cl2(1-(diphenylphosphino)-2-(diethyl)ethane)2

Base Information

Chemical Name:β-Mo2Cl2(1-(diphenylphosphino)-2-(diethyl)ethane)2
CAS No.:110373-57-4
Molecular Formula:C₃₆H₄₈Cl₄Mo₂P₄
Molecular Weight:938.364
Hs Code.:

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Chemical Property of β-Mo2Cl2(1-(diphenylphosphino)-2-(diethyl)ethane)2

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Technology Process of β-Mo2Cl2(1-(diphenylphosphino)-2-(diethyl)ethane)2

There total 2 articles about β-Mo2Cl2(1-(diphenylphosphino)-2-(diethyl)ethane)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36608-07-8
Mo₂(O₂CCF₃)4

: (1-diethylphosphino-2-diphenylphosphino)ethane

: 110373-57-4
β-Mo2Cl2(1-(diphenylphosphino)-2-(diethyl)ethane)2

Guidance literature:: With (CH₃)3SiCl; In tetrahydrofuran; dissolving Mo2(O2CCF3)4 in THF, addn. of (CH3)3SiCl, stirring for 12 h, addn. of ligand, storage for 10 h, evaporation of solvent;; washing with methanol and cold ether, drying in vac.; pure β-form from silica gel column chromatography;;

Reference yield:

: tetrapotassium octachlorodimolybdate(II)

: (1-diethylphosphino-2-diphenylphosphino)ethane

: 110373-57-4
α-Mo2Cl4(1-(diethylphosphino)-2-(diphenylphosphino)ethane)2

Guidance literature:: In methanol; refluxing mixt. of K4Mo2Cl8 and ligand in methanol for 3 h, filtration;; washing once with methanol and diethyl ether, drying in vac.; pure α-form obtained from silica gel column chromatography;;