C₂₆H₂₈N₂O₃

Base Information

Chemical Name:C₂₆H₂₈N₂O₃
CAS No.:735287-99-7
Molecular Formula:C₂₆H₂₈N₂O₃
Molecular Weight:416.52
Hs Code.:

C<sub>26</sub>H<sub>28</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₂₈N₂O₃

Chemical Property:

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Technology Process of C₂₆H₂₈N₂O₃

There total 9 articles about C₂₆H₂₈N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 380893-63-0
C₁₉H₂₄BrNO₃

: 126747-14-6
4-cyanophenylboronic acid

: 735287-99-7
C₂₆H₂₈N₂O₃

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; at 100 ℃;
DOI:10.1016/j.bmcl.2012.01.138

Reference yield:

: C₁₄H₂₁ClO₃

: 735287-99-7
C₂₆H₂₈N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride

2: titanium(IV) isopropylate; lithium hexamethyldisilazane

3: (2R,8aS)-(+)-(camphorylsulfonyl)oxaziridine; lithium hexamethyldisilazane

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water; toluene / 100 °C

With titanium(IV) isopropylate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; (2R,8aS)-(+)-(camphorylsulfonyl)oxaziridine; tri-n-butyl-tin hydride; lithium hexamethyldisilazane; In ethanol; water; toluene; 4: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.01.138

Reference yield:

: (1R,3aR,4aS,8aS,9S,9aS)-decahydro-1-methyl-3-oxo-3H-thiopyrano[3,4-f]isobenzofuran-9-carboxaldehyde

: 735287-99-7
C₂₆H₂₈N₂O₃

Guidance literature:: Multi-step reaction with 6 steps

1: sodium tetrahydroborate / methanol

2: Raney nickel / tetrahydrofuran; methanol / Reflux

3: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / Molecular sieve

4: titanium(IV) isopropylate; lithium hexamethyldisilazane

5: (2R,8aS)-(+)-(camphorylsulfonyl)oxaziridine; lithium hexamethyldisilazane

6: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water; toluene / 100 °C

With titanium(IV) isopropylate; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrapropylammonium perruthennate; (2R,8aS)-(+)-(camphorylsulfonyl)oxaziridine; 4-methylmorpholine N-oxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; ethanol; water; toluene; 6: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.01.138