3-<<oxy>methyl>thiochromate 1,1-dioxide

Base Information

Chemical Name:3-<<oxy>methyl>thiochromate 1,1-dioxide
CAS No.:77694-67-8
Molecular Formula:C₂₄H₁₈N₂O₆S
Molecular Weight:462.483
Hs Code.:

3-<<<N-(N-phenylcarbamoyl)-N-phenylcarbamoyl>oxy>methyl>thiochromate 1,1-dioxide

Synonyms:

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Chemical Property of 3-<<oxy>methyl>thiochromate 1,1-dioxide

Chemical Property:

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Technology Process of 3-<<oxy>methyl>thiochromate 1,1-dioxide

There total 4 articles about 3-<<oxy>methyl>thiochromate 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 103-71-9
phenyl isocyanate

: 77694-65-6
3-(hydroxymethyl)thiochromate 1,1-dioxide

: 77694-67-8
3-<<oxy>methyl>thiochromate 1,1-dioxide

Guidance literature:: With air; for 5h; Heating;
DOI:10.1021/jm00139a017

Reference yield:

: 491-39-4
thiochromen-4-one

: 77694-67-8
3-<<oxy>methyl>thiochromate 1,1-dioxide

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / m-cloroperbenzoic acid / CH₂Cl₂ / 3 h / 10 °C

2: 62 percent / HCl / acetic acid / Ambient temperature

3: 65 percent / 50percent formic acid, sodium formate, H₂O / 12 h / 95 °C

4: 20 percent / air / 5 h / Heating

With hydrogenchloride; formic acid; air; water; sodium formate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetic acid;
DOI:10.1021/jm00139a017

Reference yield:

: 22810-27-1
1-thiochromone 1,1-dioxide

: 77694-67-8
3-<<oxy>methyl>thiochromate 1,1-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / HCl / acetic acid / Ambient temperature

2: 65 percent / 50percent formic acid, sodium formate, H₂O / 12 h / 95 °C

3: 20 percent / air / 5 h / Heating

With hydrogenchloride; formic acid; air; water; sodium formate; In acetic acid;
DOI:10.1021/jm00139a017