bis[4-(2,6-diisopropylphenylimino)-3,3-dimethylpent-1-en-2-olato](η1-CH2Ph)2Ni2

Base Information

Chemical Name:bis[4-(2,6-diisopropylphenylimino)-3,3-dimethylpent-1-en-2-olato](η1-CH2Ph)2Ni2
CAS No.:1158506-61-6
Molecular Formula:C₅₂H₇₀N₂Ni₂O₂
Molecular Weight:872.52
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis[4-(2,6-diisopropylphenylimino)-3,3-dimethylpent-1-en-2-olato](η1-CH2Ph)2Ni2

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Technology Process of bis[4-(2,6-diisopropylphenylimino)-3,3-dimethylpent-1-en-2-olato](η1-CH2Ph)2Ni2

There total 1 articles about bis[4-(2,6-diisopropylphenylimino)-3,3-dimethylpent-1-en-2-olato](η1-CH2Ph)2Ni2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: (η3-benzyl)chloro(trimethylphosphine)nickel(II)

: 1158506-57-0
potassium 4-(2,6-diisopropylphenylimino)-3,3-dimethyl-pent-2-en-2-olate

: 1158506-61-6
bis[4-(2,6-diisopropylphenylimino)-3,3-dimethylpent-1-en-2-olato](η1-CH2Ph)2Ni2

Guidance literature:: In diethyl ether; (inert atm., Schlenk) K-salt in diethyl ether was added dropwise to a diethyl ether soln. of Ni-complex at room temp., the mixt. was stirred at room temp. overnight; cooled in freezer, decanted, the solid was washed with cold diethyl ether, dried in vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2008.12.038