Pyrrolidine, 3-(3-nitrophenyl)-1-(phenylmethyl)-

Base Information

Chemical Name:Pyrrolidine, 3-(3-nitrophenyl)-1-(phenylmethyl)-
CAS No.:145104-99-0
Molecular Formula:C17H18N2O2
Molecular Weight:282.342
Hs Code.:
DSSTox Substance ID:DTXSID20473257
Mol file:145104-99-0.mol

Synonyms:1-benzyl-3-(3-nitrophenyl)pyrrolidine;145104-99-0;PYRROLIDINE, 3-(3-NITROPHENYL)-1-(PHENYLMETHYL)-;SCHEMBL4190305;DTXSID20473257;AKOS015899448

Suppliers and Price of Pyrrolidine, 3-(3-nitrophenyl)-1-(phenylmethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Pyrrolidine, 3-(3-nitrophenyl)-1-(phenylmethyl)-

Chemical Property:

Boiling Point:405.5 °C at 760 mmHg
Flash Point:199.1 °C
Density:1.206 g/cm³
XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:282.136827821
Heavy Atom Count:21
Complexity:349

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CN(CC1C2=CC(=CC=C2)[N+](=O)[O-])CC3=CC=CC=C3

Technology Process of Pyrrolidine, 3-(3-nitrophenyl)-1-(phenylmethyl)-

There total 2 articles about Pyrrolidine, 3-(3-nitrophenyl)-1-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 586-39-0,51209-60-0
1-nitro-3-vinyl-benzene

: 93102-05-7
N-benzyl-N-(methoxymethyl)-N-[(trimethylsilyl)methyl]amine

: 145104-99-0
1-benzyl-3-(3-nitrophenyl)pyrrolidine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 16.5h;

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 145104-99-0
1-benzyl-3-(3-nitrophenyl)pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / 1,4-dioxane / 17 h / 20 - 110 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 16.5 h / 0 - 20 °C

With potassium carbonate; trifluoroacetic acid; In 1,4-dioxane; dichloromethane;