benzyl (Z)-2-phenyl-1-aminocyclopropane-1-carboxylate hydrochloride

Base Information

Chemical Name:benzyl (Z)-2-phenyl-1-aminocyclopropane-1-carboxylate hydrochloride
CAS No.:82112-07-0
Molecular Formula:C₁₇H₁₇NO₂*ClH
Molecular Weight:303.788
Hs Code.:

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Chemical Property of benzyl (Z)-2-phenyl-1-aminocyclopropane-1-carboxylate hydrochloride

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Technology Process of benzyl (Z)-2-phenyl-1-aminocyclopropane-1-carboxylate hydrochloride

There total 9 articles about benzyl (Z)-2-phenyl-1-aminocyclopropane-1-carboxylate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 87483-12-3
Benzyl (Z)-1-phthalimido-2-phenylcyclopropanecarboxylate

: 82112-07-0,87483-13-4
benzyl (Z)-2-phenyl-1-aminocyclopropane-1-carboxylate hydrochloride

Guidance literature:: With hydrogenchloride; hydrazine hydrate; 1) MeOH, room temp., 30 min, 2) steam bath, 15 min;
DOI:10.1021/jo00172a061

Reference yield:

: 17606-70-1,5839-91-8
(4Z)-4-benzylidene-2-phenyl-1,3-oxazol-5(4H)-one

: 82112-07-0,87483-13-4
benzyl (Z)-2-phenyl-1-aminocyclopropane-1-carboxylate hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / HBr (gas) / aq. HBr

2: 54 percent / CH₂Cl₂; diethyl ether / Ambient temperature

3: 74 percent / 4-(dimethylamino)pyridine / tetrahydrofuran / 48 h / Ambient temperature

4: 1.) triethyloxonium tetrafluoroborate, 2.) 1 N aq. HCl / 1.) CH₂Cl₂, reflux, overnight, 2.) room temperature, 30 min

With hydrogenchloride; dmap; hydrogen bromide; triethyloxonium fluoroborate; In tetrahydrofuran; diethyl ether; dichloromethane; hydrogen bromide;
DOI:10.1021/jo00138a014

Reference yield:

: 87483-09-8
(Z)-2-(o-Carboxyphenyl)-4-benzylidene-5-oxazolone

: 82112-07-0,87483-13-4
benzyl (Z)-2-phenyl-1-aminocyclopropane-1-carboxylate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 33 percent / CH₂Cl₂; diethyl ether / 24 h / Ambient temperature

2: 68 percent / DMAP / 2.5 h / Ambient temperature

3: 63 percent / 1) hydrazine hydrate, 2) 1 N HCl / 1) MeOH, room temp., 30 min, 2) steam bath, 15 min

With hydrogenchloride; dmap; hydrazine hydrate; In diethyl ether; dichloromethane;
DOI:10.1021/jo00172a061