((C₆H₅)2CNCH₂CH₂NC(C₆H₅)2)Fe(CH₂Si(CH₃)3)(C₆F₅)

Base Information

• Chemical Name: ((C₆H₅)2CNCH₂CH₂NC(C₆H₅)2)Fe(CH₂Si(CH₃)3)(C₆F₅)
• CAS No.: 1093215-20-3
• Molecular Formula: C₃₈H₃₅F₅FeN₂Si
• Molecular Weight: 698.634
• Mol file: 1093215-20-3.mol

Synonyms:

Chemical Property of ((C₆H₅)2CNCH₂CH₂NC(C₆H₅)2)Fe(CH₂Si(CH₃)3)(C₆F₅)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ((C₆H₅)2CNCH₂CH₂NC(C₆H₅)2)Fe(CH₂Si(CH₃)3)(C₆F₅)

There total 4 articles about ((C₆H₅)2CNCH₂CH₂NC(C₆H₅)2)Fe(CH₂Si(CH₃)3)(C₆F₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

cyclohexane (110-82-7,25012-93-5) + ((C6H5)2CNCH2CH2NC(C6H5)2)Fe(CH2Si(CH3)3)2 (1093215-22-5) + tris(pentafluorophenyl)borate (1109-15-5) → ((C6H5)2CNCH2CH2NC(C6H5)2)Fe(CH2Si(CH3)3)(C6F5) (1093215-20-3) + ((C6H5)2CNCH2CH2NC(C6H5)2)2Fe(2+)*2(CH3)3SiCH2B(C6F5)3(1-)*99C6H12=C100H70B2F30FeN4Si2*99C6H12

Guidance literature:

In toluene; mixt. of Fe complex, B(C6F5)3 and toluene stirred at 50°C for 2 d; filtered; solid washed with toluene, recrystd. from CH2Cl2-cyclohexane; filtrate combined with toluene washings, solvent removed in vac.; extd. with pentane; crystd. at -30°C (small amt. of Fe-C6F5 complex); elem. anal.;

DOI:10.1021/om8006773

Reference yield:

N,N'-bis(α-phenylbenzylidene)ethylenediamine (64042-50-8) → ((C6H5)2CNCH2CH2NC(C6H5)2)Fe(CH2Si(CH3)3)(C6F5) (1093215-20-3)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene

2: toluene

In toluene;

DOI:10.1021/om8006773

Reference yield:

((C6H5)2CNCH2CH2NC(C6H5)2)FeBr2 (1093215-12-3) → ((C6H5)2CNCH2CH2NC(C6H5)2)Fe(CH2Si(CH3)3)(C6F5) (1093215-20-3)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene-d6

2: toluene

In benzene-d6; toluene;

DOI:10.1021/om8006773

upstream raw materials:

cyclohexane

((C₆H₅)2CNCH₂CH₂NC(C₆H₅)2)Fe(CH₂Si(CH₃)3)2

tris(pentafluorophenyl)borate

N,N'-bis(α-phenylbenzylidene)ethylenediamine