Sodium; (2S,3S,4S,5R,6S)-3,4,5-trihydroxy-6-((8R,9S,13S,14S)-3-methoxy-13-methyl-17-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-2-yloxy)-tetrahydro-pyran-2-carboxylate

Base Information

Chemical Name:Sodium; (2S,3S,4S,5R,6S)-3,4,5-trihydroxy-6-((8R,9S,13S,14S)-3-methoxy-13-methyl-17-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-2-yloxy)-tetrahydro-pyran-2-carboxylate
CAS No.:116382-70-8
Molecular Formula:C₂₅H₃₁O₉*Na
Molecular Weight:498.506
Hs Code.:

Sodium; (2S,3S,4S,5R,6S)-3,4,5-trihydroxy-6-((8R,9S,13S,14S)-3-methoxy-13-methyl-17-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-2-yloxy)-tetrahydro-pyran-2-carboxylate

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Chemical Property of Sodium; (2S,3S,4S,5R,6S)-3,4,5-trihydroxy-6-((8R,9S,13S,14S)-3-methoxy-13-methyl-17-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-2-yloxy)-tetrahydro-pyran-2-carboxylate

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Technology Process of Sodium; (2S,3S,4S,5R,6S)-3,4,5-trihydroxy-6-((8R,9S,13S,14S)-3-methoxy-13-methyl-17-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-2-yloxy)-tetrahydro-pyran-2-carboxylate

There total 5 articles about Sodium; (2S,3S,4S,5R,6S)-3,4,5-trihydroxy-6-((8R,9S,13S,14S)-3-methoxy-13-methyl-17-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-2-yloxy)-tetrahydro-pyran-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116382-66-2
4-bromo-2,3-dihydroxy-1,3,5⁽¹⁰⁾-estratrien-17-one

: 116382-70-8
Sodium; (2S,3S,4S,5R,6S)-3,4,5-trihydroxy-6-((8R,9S,13S,14S)-3-methoxy-13-methyl-17-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-2-yloxy)-tetrahydro-pyran-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 79 mg / cadmium carbonate / toluene / Heating

2: 38 mg / hydrogen / palladium/charcoal / ethanol / 0.5 h / Ambient temperature

3: 4.5 mg / 2 N NaOH / methanol / 12 h / Ambient temperature

4: methanol; diethyl ether / 12 h / Ambient temperature

With sodium hydroxide; cadmium(II) carbonate; hydrogen; palladium on activated charcoal; In methanol; diethyl ether; ethanol; toluene;
DOI:10.1248/cpb.36.419

Reference yield:

: 88623-44-3
2-Amino-4-bromo-3-hydroxy-1,3,5⁽¹⁰⁾-estratrien-17-one

: 116382-70-8
Sodium; (2S,3S,4S,5R,6S)-3,4,5-trihydroxy-6-((8R,9S,13S,14S)-3-methoxy-13-methyl-17-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-2-yloxy)-tetrahydro-pyran-2-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: 175 mg / sodium metaperiodate, 0.1 N HCl / acetic acid / 0.08 h / Ambient temperature

2: 79 mg / cadmium carbonate / toluene / Heating

3: 38 mg / hydrogen / palladium/charcoal / ethanol / 0.5 h / Ambient temperature

4: 4.5 mg / 2 N NaOH / methanol / 12 h / Ambient temperature

5: methanol; diethyl ether / 12 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium periodate; cadmium(II) carbonate; hydrogen; palladium on activated charcoal; In methanol; diethyl ether; ethanol; acetic acid; toluene;
DOI:10.1248/cpb.36.419

Reference yield:

: 116382-67-3
methyl (4-bromo-3-hydroxy-17-oxo-1,3,5(10)-estratrien-2-yl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)uronate

: 116382-70-8
Sodium; (2S,3S,4S,5R,6S)-3,4,5-trihydroxy-6-((8R,9S,13S,14S)-3-methoxy-13-methyl-17-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-2-yloxy)-tetrahydro-pyran-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 38 mg / hydrogen / palladium/charcoal / ethanol / 0.5 h / Ambient temperature

2: 4.5 mg / 2 N NaOH / methanol / 12 h / Ambient temperature

3: methanol; diethyl ether / 12 h / Ambient temperature

With sodium hydroxide; hydrogen; palladium on activated charcoal; In methanol; diethyl ether; ethanol;
DOI:10.1248/cpb.36.419