Glycine, N-[N-[N-[1-[N-[1-[N-[[(4-methoxyphenyl)methoxy]carbonyl]-L-valyl]-L-prol yl]-L-leucyl]-L-prolyl]-L-alanyl]glycyl]-, hydrazide

Base Information

Chemical Name:Glycine, N-[N-[N-[1-[N-[1-[N-[[(4-methoxyphenyl)methoxy]carbonyl]-L-valyl]-L-prol yl]-L-leucyl]-L-prolyl]-L-alanyl]glycyl]-, hydrazide
CAS No.:100007-48-5
Molecular Formula:C37H57N9O10
Molecular Weight:787.914
Hs Code.:
Mol file:100007-48-5.mol

Synonyms:

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Chemical Property of Glycine, N-[N-[N-[1-[N-[1-[N-[[(4-methoxyphenyl)methoxy]carbonyl]-L-valyl]-L-prol yl]-L-leucyl]-L-prolyl]-L-alanyl]glycyl]-, hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Glycine, N-[N-[N-[1-[N-[1-[N-[[(4-methoxyphenyl)methoxy]carbonyl]-L-valyl]-L-prol yl]-L-leucyl]-L-prolyl]-L-alanyl]glycyl]-, hydrazide

There total 14 articles about Glycine, N-[N-[N-[1-[N-[1-[N-[[(4-methoxyphenyl)methoxy]carbonyl]-L-valyl]-L-prol yl]-L-leucyl]-L-prolyl]-L-alanyl]glycyl]-, hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 108304-92-3
Z(OMe)-Val-Pro-Leu-Pro-Ala-Gly-Gly-OMe

: 100007-48-5
Z(OMe)-Val-Pro-Leu-Pro-Ala-Gly-Gly-NHNH₂

Guidance literature:: With hydrazine hydrate; In methanol;
DOI:10.1248/cpb.34.2462

Reference yield:

: 23235-00-9
Z(OMe)-Val-OSu

: 100007-48-5
Z(OMe)-Val-Pro-Leu-Pro-Ala-Gly-Gly-NHNH₂

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / Et₃N / dimethylformamide / 48 h / Ambient temperature

2: 96 percent / 80 percent hydrazine hydrate / methanol

With hydrazine hydrate; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.34.2462

Reference yield:

: 53308-58-0
Z(OMe)-Pro-ONP

: 100007-48-5
Z(OMe)-Val-Pro-Leu-Pro-Ala-Gly-Gly-NHNH₂

Guidance literature:: Multi-step reaction with 8 steps

1: 94 percent / Et₃N / dimethylformamide / Ambient temperature

2: TFA, anisole / 1 h / ice-bath

3: 91 percent / Et₃N / dimethylformamide / Ambient temperature

4: TFA, anisole / 1 h / ice-bath

5: 95 percent / Et₃N / dimethylformamide / Ambient temperature

6: TFA, anisole / 1 h / ice-bath

7: 76 percent / Et₃N / dimethylformamide / 48 h / Ambient temperature

8: 96 percent / 80 percent hydrazine hydrate / methanol

With hydrazine hydrate; methoxybenzene; triethylamine; trifluoroacetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.34.2462