ferrocenyl(benzyl)benzimidazole

Base Information

• Chemical Name: ferrocenyl(benzyl)benzimidazole
• CAS No.: 654083-54-2
• Molecular Formula: C₂₄H₂₀FeN₂
• Molecular Weight: 392.283
• Mol file: 654083-54-2.mol

Synonyms:

Chemical Property of ferrocenyl(benzyl)benzimidazole

Chemical Property:

Purity/Quality:

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Technology Process of ferrocenyl(benzyl)benzimidazole

There total 1 articles about ferrocenyl(benzyl)benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

1-ferrocenylphenylmethanol + 1,1'-sulfinylbisbenzimidazole (76113-59-2) → ferrocenyl(benzyl)benzimidazole (654083-54-2)

Guidance literature:

In dichloromethane; byproducts: benzimidazole, SO2; refluxing a mixt. of iron complex and dibenzimidazole in CH2Cl2 for 1 h,cooling; addn. of ether, washing with 20% phosphoric acid, adjusting to pH 5, extn. with CH2Cl2, drying (Na2SO4), evapn., drying over CaCl2;

DOI:10.1016/j.jorganchem.2003.08.039

upstream raw materials:

1,1'-sulfinylbisbenzimidazole