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Technology Process of [(C5H5)2Zr(N(C(CH3)3)CH(C6H4Br)CH2O)]

[(C5H5)2Zr(N(C(CH3)3)CH(C6H4Br)CH2O)]

Base Information
  • Chemical Name:[(C5H5)2Zr(N(C(CH3)3)CH(C6H4Br)CH2O)]
  • CAS No.:850352-85-1
  • Molecular Formula:C22H26BrNOZr
  • Molecular Weight:491.583
  • Hs Code.:
[(C<sub>5</sub>H<sub>5</sub>)2Zr(N(C(CH<sub>3</sub>)3)CH(C<sub>6</sub>H<sub>4</sub>Br)CH<sub>2</sub>O)]

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Chemical Property of [(C5H5)2Zr(N(C(CH3)3)CH(C6H4Br)CH2O)]
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Technology Process of [(C5H5)2Zr(N(C(CH3)3)CH(C6H4Br)CH2O)]

There total 1 articles about [(C5H5)2Zr(N(C(CH3)3)CH(C6H4Br)CH2O)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

(+/-)-2-(4-bromophenyl)oxirane
32017-76-8

(+/-)-2-(4-bromophenyl)oxirane

bis(cyclopentadienyl)(tert-butylimido)(tetrahydrofuran)zirconium(IV)

bis(cyclopentadienyl)(tert-butylimido)(tetrahydrofuran)zirconium(IV)

[(C<sub>5</sub>H<sub>5</sub>)2Zr(N(C(CH<sub>3</sub>)3)CH(C<sub>6</sub>H<sub>4</sub>Br)CH<sub>2</sub>O)]
850352-85-1

[(C5H5)2Zr(N(C(CH3)3)CH(C6H4Br)CH2O)]

Guidance literature:
In benzene; (N2); glovebox or Schlenk technique; soln. of oxide in C6H6 was added toZr complex; mixt. was reacted for 2 d; volatiles removed (vac.); taken up in ether; pentane diffused at -35°C for 6 d; mother liquor removed; washed (cold pentane); solvent dried (vac.); elem. anal.;
DOI:10.1021/om049105r
upstream raw materials:

(+/-)-2-(4-bromophenyl)oxirane

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