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[Co(2,4,9,11-tetraphenyl-6,13-dimethyl-1,5,8,12-tetraazacyclotetradeca-1,4,8,11-tetraene)(NCS)2]

Base Information
  • Chemical Name:[Co(2,4,9,11-tetraphenyl-6,13-dimethyl-1,5,8,12-tetraazacyclotetradeca-1,4,8,11-tetraene)(NCS)2]
  • CAS No.:873550-09-5
  • Molecular Formula:C38H36CoN6S2
  • Molecular Weight:699.869
  • Hs Code.:
[Co(2,4,9,11-tetraphenyl-6,13-dimethyl-1,5,8,12-tetraazacyclotetradeca-1,4,8,11-tetraene)(NCS)2]

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Chemical Property of [Co(2,4,9,11-tetraphenyl-6,13-dimethyl-1,5,8,12-tetraazacyclotetradeca-1,4,8,11-tetraene)(NCS)2]
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Technology Process of [Co(2,4,9,11-tetraphenyl-6,13-dimethyl-1,5,8,12-tetraazacyclotetradeca-1,4,8,11-tetraene)(NCS)2]

There total 1 articles about [Co(2,4,9,11-tetraphenyl-6,13-dimethyl-1,5,8,12-tetraazacyclotetradeca-1,4,8,11-tetraene)(NCS)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In ethanol; EtOH soln. of the ligand (0.002 mol) was added to an EtOH soln. of Co(II)-contg. compd. (0.002 mol); soln. was refluxed on a water bath at 70-80°C for 7-8 h; the soln. was concd. to half of its vol. under reduced pressure and keptovernight at ca. 5°C; the crystals were filtered, washed with Et OH and dried under vac. over P4O10; elem. anal.;
DOI:10.1016/j.saa.2005.04.002
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