8-<(4-amino-1-methylbutyl)amino>-6-methoxy-4-(methoxymethyl)-5-quinoline phosphate

Base Information

Chemical Name:8-<(4-amino-1-methylbutyl)amino>-6-methoxy-4-(methoxymethyl)-5-quinoline phosphate
CAS No.:98510-04-4
Molecular Formula:C₂₄H₂₈F₃N₃O₃*H₃O₄P
Molecular Weight:561.495
Hs Code.:

8-<(4-amino-1-methylbutyl)amino>-6-methoxy-4-(methoxymethyl)-5-<m-(trifluoromethyl)phenoxy>quinoline phosphate

Synonyms:

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Chemical Property of 8-<(4-amino-1-methylbutyl)amino>-6-methoxy-4-(methoxymethyl)-5-quinoline phosphate

Chemical Property:

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Technology Process of 8-<(4-amino-1-methylbutyl)amino>-6-methoxy-4-(methoxymethyl)-5-quinoline phosphate

There total 7 articles about 8-<(4-amino-1-methylbutyl)amino>-6-methoxy-4-(methoxymethyl)-5-quinoline phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63460-47-9
2-(4-iodopentyl)-1,3-isoindolinedione

: 98510-04-4
8-<(4-amino-1-methylbutyl)amino>-6-methoxy-4-(methoxymethyl)-5-quinoline phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dimethylformamide / 90 °C

2: 1.) hydrazine, 2.) phosphoric acid / 1.) ethanol, 60 deg C, 4 h, 2.) ethanol

With phosphoric acid; triethylamine; hydrazine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00149a004

Reference yield:

: 82333-37-7
6-methoxy-4-methyl-8-nitro-5-<3-(trifluoromethyl)phenoxy>quinoline

: 98510-04-4
8-<(4-amino-1-methylbutyl)amino>-6-methoxy-4-(methoxymethyl)-5-quinoline phosphate

Guidance literature:: Multi-step reaction with 6 steps

1: 81 percent / acetic acid, selenium dioxide / dioxane; acetic anhydride / Heating

2: 88 percent / sodium borohydride / tetrahydrofuran; ethanol / 1 h

3: 70 percent / ethyltributylammonium iodide, potassium hydroxide / tetrahydrofuran; H₂O / 23 h

4: 2N hydrochloric acid, stannous chloride, tin / tetrahydrofuran; ethanol / 1 h / 5 - 10 °C

5: triethylamine / dimethylformamide / 90 °C

6: 1.) hydrazine, 2.) phosphoric acid / 1.) ethanol, 60 deg C, 4 h, 2.) ethanol

With hydrogenchloride; potassium hydroxide; tin; sodium tetrahydroborate; selenium(IV) oxide; phosphoric acid; tributylethylammonium iodide; acetic acid; triethylamine; tin(ll) chloride; hydrazine; In tetrahydrofuran; 1,4-dioxane; ethanol; water; acetic anhydride; N,N-dimethyl-formamide;
DOI:10.1021/jm00149a004

Reference yield:

: 98510-01-1
8-amino-6-methoxy-4-(methoxymethyl)-5-quinoline

: 98510-04-4
8-<(4-amino-1-methylbutyl)amino>-6-methoxy-4-(methoxymethyl)-5-quinoline phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dimethylformamide / 90 °C

2: 1.) hydrazine, 2.) phosphoric acid / 1.) ethanol, 60 deg C, 4 h, 2.) ethanol

With phosphoric acid; triethylamine; hydrazine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00149a004