(RS)-N¹-<6-<alanyl>amino>hexanoyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

Base Information

Chemical Name:(RS)-N¹-<6-<alanyl>amino>hexanoyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin
CAS No.:150746-73-9
Molecular Formula:C₄₂H₅₅N₅O₇S₂
Molecular Weight:806.06
Hs Code.:

(RS)-N<sup>1</sup>-<6-<<N-<(Naphth-1-yl)acetyl>alanyl>amino>hexanoyl>-N<sup>4</sup>,N<sup>8</sup>-bis(toluol-4-sulfonyl)spermidin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (RS)-N¹-<6-<alanyl>amino>hexanoyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

Chemical Property:

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Technology Process of (RS)-N¹-<6-<alanyl>amino>hexanoyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

There total 3 articles about (RS)-N¹-<6-<alanyl>amino>hexanoyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 150671-87-7
N¹-<6-<(Benzyloxycarbonyl)amino>hexanoyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

: 150746-73-9
(RS)-N¹-<6-<alanyl>amino>hexanoyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / H₂ / 10percent Pd/C / methanol / 24 h / 760 Torr

2: 1) 1,1'-carbonyldiimidazole / 1) THF, r.t, 2 h, 2) r.t., 1 h

With hydrogen; 1,1'-carbonyldiimidazole; palladium on activated charcoal; In methanol;
DOI:10.1002/hlca.19930760304

Reference yield:

: 86-87-3
naphth-1-yl acetic acid

: 150746-73-9
(RS)-N¹-<6-<alanyl>amino>hexanoyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / 2N NaOH / CH₂Cl₂ / 0.5 h / 20 °C

2: 1) 1,1'-carbonyldiimidazole / 1) THF, r.t, 2 h, 2) r.t., 1 h

With sodium hydroxide; 1,1'-carbonyldiimidazole; In dichloromethane;
DOI:10.1002/hlca.19930760304

Reference yield:

: 150671-94-6
N-<(Naphth-1-yl)acetyl>-Dl-alanin

: 150671-90-2
N¹-(6-Aminohexanoyl)-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

: 150746-73-9
(RS)-N¹-<6-<alanyl>amino>hexanoyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

Guidance literature:: With 1,1'-carbonyldiimidazole; Yield given. Multistep reaction; 1) THF, r.t, 2 h, 2) r.t., 1 h;
DOI:10.1002/hlca.19930760304