4-Oxalyl-isophthalic acid

Base Information

Chemical Name:4-Oxalyl-isophthalic acid
CAS No.:56072-59-4
Molecular Formula:C₁₀H₆O₇
Molecular Weight:238.153
Hs Code.:

Synonyms:

Suppliers and Price of 4-Oxalyl-isophthalic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-Oxalyl-isophthalic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-Oxalyl-isophthalic acid

There total 1 articles about 4-Oxalyl-isophthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89-74-7
2,4-dimethylacetophenone.

: 56072-59-4
4-Oxalyl-isophthalic acid

Guidance literature:: With potassium permanganate; potassium carbonate; In water; at 70 ℃; for 2h;
DOI:10.1248/cpb.33.2809

Reference yield:

: 56072-59-4
4-Oxalyl-isophthalic acid

: 103286-34-6
7-amino-2-phenyl-1(2H)-phthalazinone

Guidance literature:: Multi-step reaction with 5 steps

1: aq. HCl / Heating

2: H₂O / 15 h / Ambient temperature

3: 1.) ClCO₂Et, Et₃N; 2.) NaN₃

4: 72 percent / benzene / 6 h / 90 °C / Heating

5: 86 percent / H₂ / 10 percent palladium carbon / dioxane / Ambient temperature

With hydrogenchloride; sodium azide; hydrogen; chloroformic acid ethyl ester; triethylamine; palladium carbon; In 1,4-dioxane; water; benzene;
DOI:10.1248/cpb.33.2809

Reference yield:

: 56072-59-4
4-Oxalyl-isophthalic acid

: 103286-48-2
7-dimethylamino-2-phenyl-1(2H)-phthalazinone

Guidance literature:: Multi-step reaction with 6 steps

1: aq. HCl / Heating

2: H₂O / 15 h / Ambient temperature

3: 1.) ClCO₂Et, Et₃N; 2.) NaN₃

4: 72 percent / benzene / 6 h / 90 °C / Heating

5: 86 percent / H₂ / 10 percent palladium carbon / dioxane / Ambient temperature

6: 45 percent / NaH / tetrahydrofuran / 4 h / Heating

With hydrogenchloride; sodium azide; hydrogen; chloroformic acid ethyl ester; sodium hydride; triethylamine; palladium carbon; In tetrahydrofuran; 1,4-dioxane; water; benzene;
DOI:10.1248/cpb.33.2809