16-demethoxypyrodelphinine

Base Information

Chemical Name:16-demethoxypyrodelphinine
CAS No.:83705-18-4
Molecular Formula:C₃₀H₃₉NO₆
Molecular Weight:509.643
Hs Code.:

Synonyms:

Suppliers and Price of 16-demethoxypyrodelphinine

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Chemical Property of 16-demethoxypyrodelphinine

Chemical Property:

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Technology Process of 16-demethoxypyrodelphinine

There total 4 articles about 16-demethoxypyrodelphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60158-63-6
isopyrodelphinine

: 83705-18-4
16-demethoxypyrodelphinine

Guidance literature:: Multi-step reaction with 2 steps

1: 242 mg / H₂ / 10percent Pd/C / acetic acid / 42 h / 2660 Torr

2: 173 mg / 0.08 h / 220 - 230 °C / 0.01 Torr

With hydrogen; palladium on activated charcoal; In acetic acid;
DOI:10.1021/jo00148a012

Reference yield:

: 60050-12-6
pyrodelphinine

: 83705-18-4
16-demethoxypyrodelphinine

Guidance literature:: Multi-step reaction with 3 steps

1: 146 mg / TsOH / 1.) RT, 30 min, 2.) 70-80 deg C, 1 h

2: 242 mg / H₂ / 10percent Pd/C / acetic acid / 42 h / 2660 Torr

3: 173 mg / 0.08 h / 220 - 230 °C / 0.01 Torr

With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In acetic acid;
DOI:10.1021/jo00148a012

Reference yield:

: 561-07-9
delphinine

: 83705-18-4
16-demethoxypyrodelphinine

Guidance literature:: Multi-step reaction with 4 steps

1: 220 mg / 0.12 h / 230 - 240 °C / 0.01 Torr

2: 146 mg / TsOH / 1.) RT, 30 min, 2.) 70-80 deg C, 1 h

3: 242 mg / H₂ / 10percent Pd/C / acetic acid / 42 h / 2660 Torr

4: 173 mg / 0.08 h / 220 - 230 °C / 0.01 Torr

With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In acetic acid;
DOI:10.1021/jo00148a012