2,4-bis-methylsulfanyl-aniline

Base Information

Chemical Name:2,4-bis-methylsulfanyl-aniline
CAS No.:57946-71-1
Molecular Formula:C₈H₁₁NS₂
Molecular Weight:185.314
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-bis-methylsulfanyl-aniline

Chemical Property:

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Technology Process of 2,4-bis-methylsulfanyl-aniline

There total 3 articles about 2,4-bis-methylsulfanyl-aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₇H₆FNO₂S

: 57946-71-1
2,4-bis-methylsulfanyl-aniline

Guidance literature:: Multi-step reaction with 2 steps

1: isopropyl alcohol; water / 12 h / 20 °C

2: acetic acid; iron / ethyl acetate / 3 h / 60 - 80 °C

With iron; acetic acid; In water; ethyl acetate; isopropyl alcohol;
DOI:10.1021/acs.joc.1c02747

Reference yield:

: 70019-41-9
4-chloro-2-(methylthio)-1-nitrobenzene

: 57946-71-1
2,4-bis-methylsulfanyl-aniline

Guidance literature:: Multi-step reaction with 3 steps

1: diluted alcohol; sodium disulfide

2: sodium sulfide; aqueous-alcoholic NaOH-solution / Behandeln des Reaktiosprodukts mit Dimethylsulfat

3: tin; hydrochloric acid; glacial acetic acid

With hydrogenchloride; sodium sulfide; sodium hydroxide; tin; ethanol; acetic acid; sodium disulfide;

Reference yield:

: 857785-91-2
bis-(3-methylsulfanyl-4-nitro-phenyl)-disulfide

: 57946-71-1
2,4-bis-methylsulfanyl-aniline

Guidance literature:: Multi-step reaction with 2 steps

1: sodium sulfide; aqueous-alcoholic NaOH-solution / Behandeln des Reaktiosprodukts mit Dimethylsulfat

2: tin; hydrochloric acid; glacial acetic acid

With hydrogenchloride; sodium sulfide; sodium hydroxide; tin; acetic acid;