4,15-bis(4-chlorophenyl)-8,10,19,21-tetramethyl-2,4,6,8,10,13,15,17,19,21-decaazahexacyclo<10.10.0.0^1.18.0^2.6.0^7.12.0^13.17>docosan-3,5,9,11,14,16,20,22-octaone

Base Information

• Chemical Name: 4,15-bis(4-chlorophenyl)-8,10,19,21-tetramethyl-2,4,6,8,10,13,15,17,19,21-decaazahexacyclo<10.10.0.0^1.18.0^2.6.0^7.12.0^13.17>docosan-3,5,9,11,14,16,20,22-octaone
• CAS No.: 96567-07-6
• Molecular Formula: C₂₈H₂₂Cl₂N₁₀O₈
• Molecular Weight: 697.451

Synonyms:

Chemical Property of 4,15-bis(4-chlorophenyl)-8,10,19,21-tetramethyl-2,4,6,8,10,13,15,17,19,21-decaazahexacyclo<10.10.0.0^1.18.0^2.6.0^7.12.0^13.17>docosan-3,5,9,11,14,16,20,22-octaone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 4,15-bis(4-chlorophenyl)-8,10,19,21-tetramethyl-2,4,6,8,10,13,15,17,19,21-decaazahexacyclo<10.10.0.0^1.18.0^2.6.0^7.12.0^13.17>docosan-3,5,9,11,14,16,20,22-octaone

There total 3 articles about 4,15-bis(4-chlorophenyl)-8,10,19,21-tetramethyl-2,4,6,8,10,13,15,17,19,21-decaazahexacyclo<10.10.0.0^1.18.0^2.6.0^7.12.0^13.17>docosan-3,5,9,11,14,16,20,22-octaone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

5-(4-<4-chlorophenyl>-3,5-dioxo-1,2,4-triazolidin-1-yl)-1,3-dimethyluracil (96567-03-2) → 4,15-bis(4-chlorophenyl)-8,10,19,21-tetramethyl-2,4,6,8,10,13,15,17,19,21-decaazahexacyclo<10.10.0.01.18.02.6.07.12.013.17>docosan-3,5,9,11,14,16,20,22-octaone (96567-07-6)

Guidance literature:

With N-Bromosuccinimide; In chloroform; for 1h; Ambient temperature;

Reference yield:

1,3-dimethyluracil (874-14-6,156398-76-4) → 4,15-bis(4-chlorophenyl)-8,10,19,21-tetramethyl-2,4,6,8,10,13,15,17,19,21-decaazahexacyclo<10.10.0.01.18.02.6.07.12.013.17>docosan-3,5,9,11,14,16,20,22-octaone (96567-07-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / acetonitrile / Heating

2: 66 percent / NBS / CHCl₃ / 1 h / Ambient temperature

With N-Bromosuccinimide; In chloroform; acetonitrile;

Reference yield:

4-(4-chlorophenyl)-1,2,4-triazoline-3,5-dione (59068-43-8) → 4,15-bis(4-chlorophenyl)-8,10,19,21-tetramethyl-2,4,6,8,10,13,15,17,19,21-decaazahexacyclo<10.10.0.01.18.02.6.07.12.013.17>docosan-3,5,9,11,14,16,20,22-octaone (96567-07-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / acetonitrile / Heating

2: 66 percent / NBS / CHCl₃ / 1 h / Ambient temperature

With N-Bromosuccinimide; In chloroform; acetonitrile;

upstream raw materials:

5-(4-<4-chlorophenyl>-3,5-dioxo-1,2,4-triazolidin-1-yl)-1,3-dimethyluracil

1,3-dimethyluracil

4-(4-chlorophenyl)-1,2,4-triazoline-3,5-dione

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